methyl (2-azido-2-deoxy-3-O-benzyl-6-deoxy-6-phthalimido-α-D-glucopyranosyl)-(1->4)-2,6-diazido-2,6-dideoxy-3-O-benzyl-α-D-glucopyranoside

Base Information

Chemical Name:methyl (2-azido-2-deoxy-3-O-benzyl-6-deoxy-6-phthalimido-α-D-glucopyranosyl)-(1->4)-2,6-diazido-2,6-dideoxy-3-O-benzyl-α-D-glucopyranoside
CAS No.:1245566-93-1
Molecular Formula:C₃₅H₃₆N₁₀O₉
Molecular Weight:740.732
Hs Code.:

Synonyms:methyl (2-azido-2-deoxy-3-O-benzyl-6-deoxy-6-phthalimido-α-D-glucopyranosyl)-(1->4)-2,6-diazido-2,6-dideoxy-3-O-benzyl-α-D-glucopyranoside

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Chemical Property of methyl (2-azido-2-deoxy-3-O-benzyl-6-deoxy-6-phthalimido-α-D-glucopyranosyl)-(1->4)-2,6-diazido-2,6-dideoxy-3-O-benzyl-α-D-glucopyranoside

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Technology Process of methyl (2-azido-2-deoxy-3-O-benzyl-6-deoxy-6-phthalimido-α-D-glucopyranosyl)-(1->4)-2,6-diazido-2,6-dideoxy-3-O-benzyl-α-D-glucopyranoside

There total 13 articles about methyl (2-azido-2-deoxy-3-O-benzyl-6-deoxy-6-phthalimido-α-D-glucopyranosyl)-(1->4)-2,6-diazido-2,6-dideoxy-3-O-benzyl-α-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 1245566-92-0
methyl (4-O-acetyl-2-azido-2-deoxy-3-O-benzyl-6-deoxy-6-phthalimido-α-D-glucopyranosyl)-(1->4)-2,6-diazido-2,6-dideoxy-3-O-benzyl-α-D-glucopyranoside

: 1245566-93-1
methyl (2-azido-2-deoxy-3-O-benzyl-6-deoxy-6-phthalimido-α-D-glucopyranosyl)-(1->4)-2,6-diazido-2,6-dideoxy-3-O-benzyl-α-D-glucopyranoside

Guidance literature:: With acetyl chloride; In methanol; dichloromethane; for 14h; Inert atmosphere; Reflux;

Reference yield:

: 1245566-84-0
phenyl 4-O-acetyl-2-azido-2-deoxy-3-O-benzyl-6-deoxy-6-phthalimido-1-thio-β-D-glucopyranoside

: 1245566-93-1
methyl (2-azido-2-deoxy-3-O-benzyl-6-deoxy-6-phthalimido-α-D-glucopyranosyl)-(1->4)-2,6-diazido-2,6-dideoxy-3-O-benzyl-α-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: N-iodo-succinimide; trifluorormethanesulfonic acid / diethyl ether; dichloromethane / 1 h / 0 °C / Inert atmosphere

2: acetyl chloride / methanol; dichloromethane / 19 h / Reflux; Inert atmosphere

With N-iodo-succinimide; trifluorormethanesulfonic acid; acetyl chloride; In methanol; diethyl ether; dichloromethane;
DOI:10.1021/jo200951p

Reference yield:

: 1245566-89-5
C₁₅H₂₁N₃O₇S

: 1245566-93-1
methyl (2-azido-2-deoxy-3-O-benzyl-6-deoxy-6-phthalimido-α-D-glucopyranosyl)-(1->4)-2,6-diazido-2,6-dideoxy-3-O-benzyl-α-D-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: sodium azide / N,N-dimethyl-formamide / 10.5 h / 80 °C / Inert atmosphere

2: N-iodo-succinimide; trifluorormethanesulfonic acid / diethyl ether; dichloromethane / 1 h / 0 °C / Inert atmosphere

3: acetyl chloride / methanol; dichloromethane / 19 h / Reflux; Inert atmosphere

With N-iodo-succinimide; sodium azide; trifluorormethanesulfonic acid; acetyl chloride; In methanol; diethyl ether; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jo200951p