N^α-(tert-butoxycarbonyl)prolyl-O-(dimethylphosphono)tyrosylvaline

Base Information

Chemical Name:N^α-(tert-butoxycarbonyl)prolyl-O-(dimethylphosphono)tyrosylvaline
CAS No.:118903-68-7
Molecular Formula:C₂₆H₄₀N₃O₁₀P
Molecular Weight:585.591
Hs Code.:

N<sup>α</sup>-(tert-butoxycarbonyl)prolyl-O-(dimethylphosphono)tyrosylvaline

Synonyms:N^α-(tert-butoxycarbonyl)prolyl-O-(dimethylphosphono)tyrosylvaline

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N^α-(tert-butoxycarbonyl)prolyl-O-(dimethylphosphono)tyrosylvaline

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Technology Process of N^α-(tert-butoxycarbonyl)prolyl-O-(dimethylphosphono)tyrosylvaline

There total 1 articles about N^α-(tert-butoxycarbonyl)prolyl-O-(dimethylphosphono)tyrosylvaline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 118903-67-6
N^α-(tert-butoxycarbonyl)prolyl-O-(dimethylphosphono)tyrosylvaline anthraquinon-2-ylmethyl ester

: 118903-68-7
N^α-(tert-butoxycarbonyl)prolyl-O-(dimethylphosphono)tyrosylvaline

Guidance literature:: With sodium dithionite; sodium hydrogencarbonate; In 1,4-dioxane; water; for 3h;
DOI:10.1021/jo00300a041

Reference yield:

: 118903-68-7
N^α-(tert-butoxycarbonyl)prolyl-O-(dimethylphosphono)tyrosylvaline

: 118903-70-1
prolyl-O-(dimethylphosphono)tyrosylvaline trifluoroacetate

Guidance literature:: With trifluoroacetic acid; In dichloromethane; water; for 1h;
DOI:10.1021/jo00300a041

Reference yield:

: 118903-68-7
N^α-(tert-butoxycarbonyl)prolyl-O-(dimethylphosphono)tyrosylvaline

: 127103-03-1
prolyl-O-phosphotyrosylvaline trifluoroacetate

Guidance literature:: Multi-step reaction with 2 steps

1: CF₃COOH / H₂O; CH₂Cl₂ / 1 h

2: 66 percent / trifluoromethanesulfonic acid, dimethyl sulfide / trifluoroacetic acid; various solvent(s) / 4 h / 0 °C / or trimethylsilyl bromide, trimethylsilyl trifluoromethanesulfonate, thioanisole

With dimethylsulfide; trifluorormethanesulfonic acid; trifluoroacetic acid; In dichloromethane; water; trifluoroacetic acid;
DOI:10.1021/jo00300a041