2,2-Dimethyl-propionic acid (1R,2R,3S)-3-benzyloxy-1-(2,2-dimethyl-propionyloxymethyl)-2-methoxymethoxy-3-methyl-nonyl ester

Base Information

Chemical Name:2,2-Dimethyl-propionic acid (1R,2R,3S)-3-benzyloxy-1-(2,2-dimethyl-propionyloxymethyl)-2-methoxymethoxy-3-methyl-nonyl ester
CAS No.:175408-91-0
Molecular Formula:C₃₀H₅₀O₇
Molecular Weight:522.723
Hs Code.:

Synonyms:2,2-Dimethyl-propionic acid (1R,2R,3S)-3-benzyloxy-1-(2,2-dimethyl-propionyloxymethyl)-2-methoxymethoxy-3-methyl-nonyl ester

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Chemical Property of 2,2-Dimethyl-propionic acid (1R,2R,3S)-3-benzyloxy-1-(2,2-dimethyl-propionyloxymethyl)-2-methoxymethoxy-3-methyl-nonyl ester

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Technology Process of 2,2-Dimethyl-propionic acid (1R,2R,3S)-3-benzyloxy-1-(2,2-dimethyl-propionyloxymethyl)-2-methoxymethoxy-3-methyl-nonyl ester

There total 6 articles about 2,2-Dimethyl-propionic acid (1R,2R,3S)-3-benzyloxy-1-(2,2-dimethyl-propionyloxymethyl)-2-methoxymethoxy-3-methyl-nonyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 168776-32-7
(2R,3R,4S,5Z)-4-(benzyloxy)-3-(methoxymethoxy)-4-methyl-1,2-bis(pivaloyloxy)-5-decene

: 175408-91-0
2,2-Dimethyl-propionic acid (1R,2R,3S)-3-benzyloxy-1-(2,2-dimethyl-propionyloxymethyl)-2-methoxymethoxy-3-methyl-nonyl ester

Guidance literature:: With hydrogen; palladium on activated charcoal;
DOI:10.1021/jo951897z

Reference yield:

: 29541-98-8,55317-64-1
pentylidenetriphenylphosphorane

: 175408-91-0
2,2-Dimethyl-propionic acid (1R,2R,3S)-3-benzyloxy-1-(2,2-dimethyl-propionyloxymethyl)-2-methoxymethoxy-3-methyl-nonyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 91 percent / tetrahydrofuran / 0.5 h / Ambient temperature

2: 87 percent / H₂ / Pd on charcoal

With hydrogen; palladium on activated charcoal; In tetrahydrofuran;
DOI:10.1021/jo951897z

Reference yield:

: 175408-87-4
2,2-Dimethyl-propionic acid (1R,2R,3R)-3-benzyloxy-1-(2,2-dimethyl-propionyloxymethyl)-2-hydroxy-3-methyl-4-oxo-butyl ester

: 175408-91-0
2,2-Dimethyl-propionic acid (1R,2R,3S)-3-benzyloxy-1-(2,2-dimethyl-propionyloxymethyl)-2-methoxymethoxy-3-methyl-nonyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: i-Pr₂NEt / 20 h / Heating

2: 91 percent / tetrahydrofuran / 0.5 h / Ambient temperature

3: 87 percent / H₂ / Pd on charcoal

With hydrogen; N-ethyl-N,N-diisopropylamine; palladium on activated charcoal; In tetrahydrofuran;
DOI:10.1021/jo951897z