2-10-methylpteroyl)amino>tridecanedioic acid dimethyl ester

Base Information

Chemical Name:2-10-methylpteroyl)amino>tridecanedioic acid dimethyl ester
CAS No.:113976-35-5
Molecular Formula:C₃₀H₄₂N₈O₅
Molecular Weight:594.714
Hs Code.:

2-<N-(4-amino-4-deoxy-N<sup>10</sup>-methylpteroyl)amino>tridecanedioic acid dimethyl ester

Synonyms:2-10-methylpteroyl)amino>tridecanedioic acid dimethyl ester

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Chemical Property of 2-10-methylpteroyl)amino>tridecanedioic acid dimethyl ester

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Technology Process of 2-10-methylpteroyl)amino>tridecanedioic acid dimethyl ester

There total 6 articles about 2-10-methylpteroyl)amino>tridecanedioic acid dimethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: 19741-14-1
4-[(2,4-diaminopteridin-6-ylmethyl)methylamino]benzoic acid

: 113976-44-6
2-aminotridecanedioic acid dimethyl ester hydrochloride

: 113976-35-5
2-10-methylpteroyl)amino>tridecanedioic acid dimethyl ester

Guidance literature:: With diethyl cyanophosphonate; triethylamine; In N,N-dimethyl-formamide; for 76h; Ambient temperature;
DOI:10.1021/jm00402a014

Reference yield:

: 3927-59-1
tridecanedioic acid monomethyl ester

: 113976-35-5
2-10-methylpteroyl)amino>tridecanedioic acid dimethyl ester

Guidance literature:: Multi-step reaction with 6 steps

1: SOCl₂ / dimethylformamide / 3 h / Heating

2: Br₂, I₂ / SOCl₂; dimethylformamide / 4 h / Irradiation

3: 3.5 h / Ambient temperature

4: NaN₃ / ethanol / 15 h / Heating

5: H₂, aq. HCl / Pd-C / ethanol / 17 h

6: 57 percent / diethyl phosphorocyanidate, Et₃N / dimethylformamide / 76 h / Ambient temperature

With hydrogenchloride; thionyl chloride; sodium azide; diethyl cyanophosphonate; hydrogen; bromine; iodine; triethylamine; palladium on activated charcoal; In thionyl chloride; ethanol; N,N-dimethyl-formamide;
DOI:10.1021/jm00402a014

Reference yield:

: 113976-42-4
2-bromotridecanedioic acid dimethyl ester

: 113976-35-5
2-10-methylpteroyl)amino>tridecanedioic acid dimethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: NaN₃ / ethanol / 15 h / Heating

2: H₂, aq. HCl / Pd-C / ethanol / 17 h

3: 57 percent / diethyl phosphorocyanidate, Et₃N / dimethylformamide / 76 h / Ambient temperature

With hydrogenchloride; sodium azide; diethyl cyanophosphonate; hydrogen; triethylamine; palladium on activated charcoal; In ethanol; N,N-dimethyl-formamide;
DOI:10.1021/jm00402a014