C₅₀H₆₉ClN₂O₈

Base Information

Chemical Name:C₅₀H₆₉ClN₂O₈
CAS No.:1449797-80-1
Molecular Formula:C₅₀H₆₉ClN₂O₈
Molecular Weight:861.559
Hs Code.:

C<sub>50</sub>H<sub>69</sub>ClN<sub>2</sub>O<sub>8</sub>

Synonyms:C₅₀H₆₉ClN₂O₈

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Chemical Property of C₅₀H₆₉ClN₂O₈

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Technology Process of C₅₀H₆₉ClN₂O₈

There total 14 articles about C₅₀H₆₉ClN₂O₈ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 660423-00-7
4-(tert-butoxy)-3,3-dimethyl-4-oxobutanoic acid

: 1449797-79-8
C₄₀H₅₃ClN₂O₅

: 1449797-80-1
C₅₀H₆₉ClN₂O₈

Guidance literature:: With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 20 ℃;

Reference yield:

: 1449797-75-4
C₄₀H₅₃ClN₂O₆

: 1449797-80-1
C₅₀H₆₉ClN₂O₈

Guidance literature:: Multi-step reaction with 5 steps

1: N-ethyl-N,N-diisopropylamine; p-toluenesulfonyl chloride / dichloromethane / 3 h / 20 °C

2: sodium tetrahydroborate; methanol / tetrahydrofuran / 0.5 h / 0 °C

3: sodium hydroxide; water / tetrahydrofuran; methanol / 20 °C

4: triethylamine; dmap / dichloromethane / 1 h / 0 °C

5: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 20 °C

With methanol; dmap; sodium tetrahydroborate; water; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; N-ethyl-N,N-diisopropylamine; p-toluenesulfonyl chloride; sodium hydroxide; In tetrahydrofuran; methanol; dichloromethane;

Reference yield:

: 1422356-82-8
C₃₃H₄₉NO₆

: 1449797-80-1
C₅₀H₆₉ClN₂O₈

Guidance literature:: Multi-step reaction with 7 steps

1: acetic acid; sodium nitrite / dimethyl sulfoxide / 20 °C

2: N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 20 °C

3: N-ethyl-N,N-diisopropylamine; p-toluenesulfonyl chloride / dichloromethane / 3 h / 20 °C

4: sodium tetrahydroborate; methanol / tetrahydrofuran / 0.5 h / 0 °C

5: sodium hydroxide; water / tetrahydrofuran; methanol / 20 °C

6: triethylamine; dmap / dichloromethane / 1 h / 0 °C

7: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 20 °C

With methanol; dmap; sodium tetrahydroborate; water; acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; N-ethyl-N,N-diisopropylamine; p-toluenesulfonyl chloride; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; sodium hydroxide; sodium nitrite; In tetrahydrofuran; methanol; dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide;