9-hexyl-N-(9-hexyl-3-(4-(hexyloxy)phenyl)-9H-carbazol-6-yl)-6-(2-(hexyloxy)phenyl)-9H-carbazol-3-amine

Base Information

Chemical Name:9-hexyl-N-(9-hexyl-3-(4-(hexyloxy)phenyl)-9H-carbazol-6-yl)-6-(2-(hexyloxy)phenyl)-9H-carbazol-3-amine
CAS No.:1630989-46-6
Molecular Formula:C₆₀H₇₃N₃O₂
Molecular Weight:868.259
Hs Code.:

Synonyms:9-hexyl-N-(9-hexyl-3-(4-(hexyloxy)phenyl)-9H-carbazol-6-yl)-6-(2-(hexyloxy)phenyl)-9H-carbazol-3-amine

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Chemical Property of 9-hexyl-N-(9-hexyl-3-(4-(hexyloxy)phenyl)-9H-carbazol-6-yl)-6-(2-(hexyloxy)phenyl)-9H-carbazol-3-amine

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Technology Process of 9-hexyl-N-(9-hexyl-3-(4-(hexyloxy)phenyl)-9H-carbazol-6-yl)-6-(2-(hexyloxy)phenyl)-9H-carbazol-3-amine

There total 6 articles about 9-hexyl-N-(9-hexyl-3-(4-(hexyloxy)phenyl)-9H-carbazol-6-yl)-6-(2-(hexyloxy)phenyl)-9H-carbazol-3-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 156972-74-6
3-bromo-9-hexyl-9H-carbazole

: 1630989-46-6
9-hexyl-N-(9-hexyl-3-(4-(hexyloxy)phenyl)-9H-carbazol-6-yl)-6-(2-(hexyloxy)phenyl)-9H-carbazol-3-amine

Guidance literature:: Multi-step reaction with 3 steps

1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / 1,2-dimethoxyethane / Inert atmosphere; Reflux

2: N-Bromosuccinimide / N,N-dimethyl-formamide / 20 °C / Darkness

3: palladium diacetate; potassium tert-butylate / 1,2-dimethoxyethane / Inert atmosphere; Reflux

With N-Bromosuccinimide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium tert-butylate; palladium diacetate; potassium carbonate; In 1,2-dimethoxyethane; N,N-dimethyl-formamide;
DOI:10.1021/ol5018036

Reference yield:

: 1630989-85-3
9-hexyl-3-(2-(hexyloxy)phenyl)-9H-carbazole

: 1630989-46-6
9-hexyl-N-(9-hexyl-3-(4-(hexyloxy)phenyl)-9H-carbazol-6-yl)-6-(2-(hexyloxy)phenyl)-9H-carbazol-3-amine

Guidance literature:: Multi-step reaction with 2 steps

1: N-Bromosuccinimide / N,N-dimethyl-formamide / 20 °C / Darkness

2: palladium diacetate; potassium tert-butylate / 1,2-dimethoxyethane / Inert atmosphere; Reflux

With N-Bromosuccinimide; potassium tert-butylate; palladium diacetate; In 1,2-dimethoxyethane; N,N-dimethyl-formamide;
DOI:10.1021/ol5018036

Reference yield:

: 1631755-66-2
9-hexyl-3-(4-(hexyloxy)phenyl)-6-nitro-9H-carbazole

: 1630989-46-6
9-hexyl-N-(9-hexyl-3-(4-(hexyloxy)phenyl)-9H-carbazol-6-yl)-6-(2-(hexyloxy)phenyl)-9H-carbazol-3-amine

Guidance literature:: Multi-step reaction with 2 steps

1: palladium on activated charcoal; hydrogen / tetrahydrofuran / 20 °C

2: palladium diacetate; potassium tert-butylate / 1,2-dimethoxyethane / Inert atmosphere; Reflux

With palladium on activated charcoal; potassium tert-butylate; hydrogen; palladium diacetate; In tetrahydrofuran; 1,2-dimethoxyethane;
DOI:10.1021/ol5018036