di-tert-butyl 2-(2,3-bis(nitrooxy)propyl)-5,6-dimethoxy-3-methyl-1,4-phenylene dicarbonate

Base Information

Chemical Name:di-tert-butyl 2-(2,3-bis(nitrooxy)propyl)-5,6-dimethoxy-3-methyl-1,4-phenylene dicarbonate
CAS No.:1431987-55-1
Molecular Formula:C₂₂H₃₂N₂O₁₄
Molecular Weight:548.501
Hs Code.:

Synonyms:di-tert-butyl 2-(2,3-bis(nitrooxy)propyl)-5,6-dimethoxy-3-methyl-1,4-phenylene dicarbonate

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Chemical Property of di-tert-butyl 2-(2,3-bis(nitrooxy)propyl)-5,6-dimethoxy-3-methyl-1,4-phenylene dicarbonate

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Technology Process of di-tert-butyl 2-(2,3-bis(nitrooxy)propyl)-5,6-dimethoxy-3-methyl-1,4-phenylene dicarbonate

There total 6 articles about di-tert-butyl 2-(2,3-bis(nitrooxy)propyl)-5,6-dimethoxy-3-methyl-1,4-phenylene dicarbonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 1431987-54-0
di-tert-butyl 2-allyl-5,6-dimethoxy-3-methyl-1,4-phenylene dicarbonate

: 1431987-55-1
di-tert-butyl 2-(2,3-bis(nitrooxy)propyl)-5,6-dimethoxy-3-methyl-1,4-phenylene dicarbonate

Guidance literature:: With iodine; silver nitrate; In acetonitrile; at -15 - 20 ℃; for 17h;

Reference yield:

: 605-94-7
2,3-Dimethoxy-5-methyl-1,4-benzoquinone

: 1431987-55-1
di-tert-butyl 2-(2,3-bis(nitrooxy)propyl)-5,6-dimethoxy-3-methyl-1,4-phenylene dicarbonate

Guidance literature:: Multi-step reaction with 6 steps

1.1: acetic acid / 20 °C

2.1: potassium tert-butylate / tetrahydrofuran / 0.5 h / 0 °C

2.2: 2 h

3.1: toluene / 7 h / Reflux

4.1: sodium tetrahydroborate; ethanol / 0.5 h

5.1: triethylamine / tetrahydrofuran / 20 °C

6.1: silver nitrate; iodine / acetonitrile / 17 h / -15 - 20 °C

With sodium tetrahydroborate; ethanol; potassium tert-butylate; iodine; silver nitrate; acetic acid; triethylamine; In tetrahydrofuran; toluene; acetonitrile;

Reference yield:

: 2-Allyl-5,6-dimethoxy-3-methyl-benzene-1,4-diol

: 1431987-55-1
di-tert-butyl 2-(2,3-bis(nitrooxy)propyl)-5,6-dimethoxy-3-methyl-1,4-phenylene dicarbonate

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / tetrahydrofuran / 20 °C

2: silver nitrate; iodine / acetonitrile / 17 h / -15 - 20 °C

With iodine; silver nitrate; triethylamine; In tetrahydrofuran; acetonitrile;