tert-butoxycarbonylamino-(4-methoxy-benzylsulfanyl)-acetic acid methyl ester

Base Information

Chemical Name:tert-butoxycarbonylamino-(4-methoxy-benzylsulfanyl)-acetic acid methyl ester
CAS No.:892553-20-7
Molecular Formula:C₁₆H₂₃NO₅S
Molecular Weight:341.428
Hs Code.:

<i>tert</i>-butoxycarbonylamino-(4-methoxy-benzylsulfanyl)-acetic acid methyl ester

Synonyms:tert-butoxycarbonylamino-(4-methoxy-benzylsulfanyl)-acetic acid methyl ester

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Chemical Property of tert-butoxycarbonylamino-(4-methoxy-benzylsulfanyl)-acetic acid methyl ester

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Technology Process of tert-butoxycarbonylamino-(4-methoxy-benzylsulfanyl)-acetic acid methyl ester

There total 3 articles about tert-butoxycarbonylamino-(4-methoxy-benzylsulfanyl)-acetic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 892553-19-4
rac-α-(4-methoxybenzylthio)-N-(tert-butoxycarbonyl)glycine

: 18107-18-1
diazomethyl-trimethyl-silane

: 892553-20-7
tert-butoxycarbonylamino-(4-methoxy-benzylsulfanyl)-acetic acid methyl ester

Guidance literature:: In methanol; hexane; benzene; at 20 ℃; for 0.75h;
DOI:10.1021/ol0606740

Reference yield:

: 4248-19-5
tert-butyl carbazate

: 892553-20-7
tert-butoxycarbonylamino-(4-methoxy-benzylsulfanyl)-acetic acid methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 100 percent / acetone / 4 h / Heating

2: 75 percent / p-toluenesulfonic acid / benzene / 6 h / Heating

3: 99 percent / benzene; methanol; hexane / 0.75 h / 20 °C

With toluene-4-sulfonic acid; In methanol; hexane; acetone; benzene;
DOI:10.1021/ol0606740

Reference yield:

: 96625-24-0
N^α-(tert-butoxycarbonyl)-α-hydroxyglycine

: 892553-20-7
tert-butoxycarbonylamino-(4-methoxy-benzylsulfanyl)-acetic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 75 percent / p-toluenesulfonic acid / benzene / 6 h / Heating

2: 99 percent / benzene; methanol; hexane / 0.75 h / 20 °C

With toluene-4-sulfonic acid; In methanol; hexane; benzene;
DOI:10.1021/ol0606740