(1S,4S)-5-(3-(trifluoromethyl)phenyl)-5-aza-2-azoniabicyclo[2.2.1]heptane chloride

Base Information

Chemical Name:(1S,4S)-5-(3-(trifluoromethyl)phenyl)-5-aza-2-azoniabicyclo[2.2.1]heptane chloride
CAS No.:953435-74-0
Molecular Formula:C₁₂H₁₃F₃N₂*ClH
Molecular Weight:278.705
Hs Code.:

Synonyms:(1S,4S)-5-(3-(trifluoromethyl)phenyl)-5-aza-2-azoniabicyclo[2.2.1]heptane chloride

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1S,4S)-5-(3-(trifluoromethyl)phenyl)-5-aza-2-azoniabicyclo[2.2.1]heptane chloride

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Technology Process of (1S,4S)-5-(3-(trifluoromethyl)phenyl)-5-aza-2-azoniabicyclo[2.2.1]heptane chloride

There total 4 articles about (1S,4S)-5-(3-(trifluoromethyl)phenyl)-5-aza-2-azoniabicyclo[2.2.1]heptane chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 953435-75-1
(1S,4S)-tert-butyl 5-(3-(trifluoromethyl)phenyl)-2,5-diazabicyclo[2.2.1]heptane-2-carboxylate

: 953435-74-0
(1S,4S)-5-(3-(trifluoromethyl)phenyl)-5-aza-2-azoniabicyclo[2.2.1]heptane chloride

Guidance literature:: With hydrogenchloride; In 1,4-dioxane; at 0 - 20 ℃;

Reference yield: 100.0%

: 953435-74-0
(1S,4S)-5-(3-(trifluoromethyl)phenyl)-5-aza-2-azoniabicyclo[2.2.1]heptane chloride

Guidance literature:

Reference yield:

: 113451-59-5,174823-32-6
(1S,4S)-2,5-Diaza-bicyclo[2.2.1]heptane-2-carboxylic acid tert-butyl ester

: 953435-74-0
(1S,4S)-5-(3-(trifluoromethyl)phenyl)-5-aza-2-azoniabicyclo[2.2.1]heptane chloride

Guidance literature:: Multi-step reaction with 2 steps

1: bis(tri-t-butylphosphine)palladium ⁽⁰⁾; sodium t-butanolate / benzene / 110 °C / Inert atmosphere

2: hydrogenchloride / 1,4-dioxane / 0 - 20 °C

With hydrogenchloride; bis(tri-t-butylphosphine)palladium ⁽⁰⁾; sodium t-butanolate; In 1,4-dioxane; benzene;