C₂₂H₃₂N₂O₆

Base Information

Chemical Name:C₂₂H₃₂N₂O₆
CAS No.:944140-66-3
Molecular Formula:C₂₂H₃₂N₂O₆
Molecular Weight:420.506
Hs Code.:

C<sub>22</sub>H<sub>32</sub>N<sub>2</sub>O<sub>6</sub>

Synonyms:C₂₂H₃₂N₂O₆

Suppliers and Price of C₂₂H₃₂N₂O₆

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₂₂H₃₂N₂O₆

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₂₂H₃₂N₂O₆

There total 10 articles about C₂₂H₃₂N₂O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 170564-98-4
(R)-3-amino-3-phenyl-1-propanol

: (3S,5R)-1-(tert-butoxycarbonyl)-5-(methoxycarbonyl)piperidine-3-carboxylic acid

: 944140-66-3
C₂₂H₃₂N₂O₆

Guidance literature:: With 1-hydroxy-7-aza-benzotriazole; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In N,N-dimethyl-formamide; at 20 ℃; for 20h;
DOI:10.1021/ml500137b

Reference yield:

: dimethyl pyridine-3,5-dicarboxylate hydrochloride

: 944140-66-3
C₂₂H₃₂N₂O₆

Guidance literature:: Multi-step reaction with 6 steps

1: acetic acid; platinum(IV) oxide; hydrogen / 27 h / 24 °C / 3750.38 Torr / Autoclave; Large scale

2: sodium hydrogencarbonate / water; tetrahydrofuran / 20 °C / Large scale

3: potassium carbonate / water; methanol / 96 h / Reflux

4: acetic anhydride / 4.5 h / Reflux

5: hydroquinine (anthraquinone-1,4-diyl) diether / tetrahydrofuran; diethyl ether / -78 - 20 °C

6: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; 1-hydroxy-7-aza-benzotriazole / N,N-dimethyl-formamide / 20 h / 20 °C

With platinum(IV) oxide; 1-hydroxy-7-aza-benzotriazole; hydrogen; sodium hydrogencarbonate; potassium carbonate; acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; hydroquinine (anthraquinone-1,4-diyl) diether; In tetrahydrofuran; methanol; diethyl ether; water; acetic anhydride; N,N-dimethyl-formamide;
DOI:10.1021/ml500137b

Reference yield:

: dimethyl piperidine-3,5-(cis)-dicarboxylate

: 944140-66-3
C₂₂H₃₂N₂O₆

Guidance literature:: Multi-step reaction with 5 steps

1: sodium hydrogencarbonate / water; tetrahydrofuran / 20 °C / Large scale

2: potassium carbonate / water; methanol / 96 h / Reflux

3: acetic anhydride / 4.5 h / Reflux

4: hydroquinine (anthraquinone-1,4-diyl) diether / tetrahydrofuran; diethyl ether / -78 - 20 °C

5: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; 1-hydroxy-7-aza-benzotriazole / N,N-dimethyl-formamide / 20 h / 20 °C

With 1-hydroxy-7-aza-benzotriazole; sodium hydrogencarbonate; potassium carbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; hydroquinine (anthraquinone-1,4-diyl) diether; In tetrahydrofuran; methanol; diethyl ether; water; acetic anhydride; N,N-dimethyl-formamide;
DOI:10.1021/ml500137b