C₉H₇ZrCl₂C₅H₄CH₂CH₃

Base Information

• Chemical Name: C₉H₇ZrCl₂C₅H₄CH₂CH₃
• CAS No.: 638164-60-0
• Molecular Formula: C₁₆H₁₆Cl₂Zr
• Molecular Weight: 370.433
• Mol file: 638164-60-0.mol

Synonyms:C₉H₇ZrCl₂C₅H₄CH₂CH₃

Chemical Property of C₉H₇ZrCl₂C₅H₄CH₂CH₃

Chemical Property:

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Technology Process of C₉H₇ZrCl₂C₅H₄CH₂CH₃

There total 1 articles about C₉H₇ZrCl₂C₅H₄CH₂CH₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

trichloro(η5-indenyl)zirconium + ethylcyclopentadiene (22516-12-7) + ethylcyclopentadiene (22516-11-6) → C9H7ZrCl2C5H4CH2CH3 (638164-60-0)

Guidance literature:

With n-butyllithium; In diethyl ether; hexane; byproducts: n-butane, LiCl; addn. of soln. of n-BuLi in hexane to soln. of isomeric mixture of cyclopentadien derivativeat -78 °C, soln. stirred for 6 h at room temp., addn. of indenylzirconium trichloride at -78 °C, soln. stirredover night; evapn. of solvent to 50 ml, suspn. filtered with Na2SO4, extn. with CH2Cl2, concd., crystn. at -20 °C;

DOI:10.1016/S0022-328X(03)00508-4

upstream raw materials:

ethylcyclopentadiene

ethylcyclopentadiene