Technology Process of C37H53N3O9
There total 16 articles about C37H53N3O9 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sodium hydride;
In
N,N-dimethyl-formamide; mineral oil;
at 0 - 20 ℃;
for 14h;
DOI:10.1021/ja105119r
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: water; sodium hydroxide / tetrahydrofuran; methanol / 23 h
1.2: pH 1
2.1: thionyl chloride / 2 h / 85 °C
3.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 2.5 h / 0 - 20 °C
4.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 14 h / 0 - 20 °C
5.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 14 h / 0 - 20 °C
With
thionyl chloride; tetrabutyl ammonium fluoride; water; sodium hydride; N-ethyl-N,N-diisopropylamine; sodium hydroxide;
In
tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide; mineral oil;
DOI:10.1021/ja105119r
- Guidance literature:
-
Multi-step reaction with 4 steps
1: thionyl chloride / 2 h / 85 °C
2: N-ethyl-N,N-diisopropylamine / dichloromethane / 2.5 h / 0 - 20 °C
3: tetrabutyl ammonium fluoride / tetrahydrofuran / 14 h / 0 - 20 °C
4: sodium hydride / N,N-dimethyl-formamide; mineral oil / 14 h / 0 - 20 °C
With
thionyl chloride; tetrabutyl ammonium fluoride; sodium hydride; N-ethyl-N,N-diisopropylamine;
In
tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; mineral oil;
DOI:10.1021/ja105119r
