Technology Process of C18H30N2
There total 8 articles about C18H30N2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
dimethyl sulfide borane;
In
tetrahydrofuran;
at 0 ℃;
Reflux;
DOI:10.1002/ejoc.201000569
- Guidance literature:
-
Multi-step reaction with 5 steps
1: dimethyl sulfoxide / 8 h / 90 °C / Inert atmosphere
2: hydrazine hydrate / ethanol; toluene / 0 °C / Reflux
3: tetrahydrofuran / 51 h / 0 °C / Inert atmosphere; Reflux
4: trifluoroacetic acid / dichloromethane / 2 h / 0 - 20 °C
5: dimethyl sulfide borane / tetrahydrofuran / 0 °C / Reflux
With
dimethyl sulfide borane; hydrazine hydrate; trifluoroacetic acid;
In
tetrahydrofuran; ethanol; dichloromethane; dimethyl sulfoxide; toluene;
DOI:10.1002/ejoc.201000569
- Guidance literature:
-
Multi-step reaction with 4 steps
1: hydrazine hydrate / ethanol; toluene / 0 °C / Reflux
2: tetrahydrofuran / 51 h / 0 °C / Inert atmosphere; Reflux
3: trifluoroacetic acid / dichloromethane / 2 h / 0 - 20 °C
4: dimethyl sulfide borane / tetrahydrofuran / 0 °C / Reflux
With
dimethyl sulfide borane; hydrazine hydrate; trifluoroacetic acid;
In
tetrahydrofuran; ethanol; dichloromethane; toluene;
DOI:10.1002/ejoc.201000569