Technology Process of p-tolyl 3-O-allyl-2,4-di-O-(2-napthyl)methyl-1-thio-β-D-glucopyranoside
There total 4 articles about p-tolyl 3-O-allyl-2,4-di-O-(2-napthyl)methyl-1-thio-β-D-glucopyranoside which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: sodium hydride / N,N-dimethyl-formamide / 2 h / 0 - 20 °C
2: lithium aluminium tetrahydride; aluminum (III) chloride / dichloromethane; diethyl ether / 2.5 h / Reflux
With
aluminum (III) chloride; lithium aluminium tetrahydride; sodium hydride;
In
diethyl ether; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1039/c3ob42503g
- Guidance literature:
-
With
aluminum (III) chloride; lithium aluminium tetrahydride;
In
diethyl ether; dichloromethane;
for 2.5h;
Reflux;
DOI:10.1039/c3ob42503g
- Guidance literature:
-
Multi-step reaction with 3 steps
1: toluene-4-sulfonic acid / N,N-dimethyl-formamide / 3 h / 0 - 20 °C
2: sodium hydride / N,N-dimethyl-formamide / 2 h / 0 - 20 °C
3: lithium aluminium tetrahydride; aluminum (III) chloride / dichloromethane; diethyl ether / 2.5 h / Reflux
With
aluminum (III) chloride; lithium aluminium tetrahydride; sodium hydride; toluene-4-sulfonic acid;
In
diethyl ether; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1039/c3ob42503g