methyl (3β)-1-benzoyl-2,3-dihydroisolysergate

Base Information

Chemical Name:methyl (3β)-1-benzoyl-2,3-dihydroisolysergate
CAS No.:62592-69-2
Molecular Formula:C₂₄H₂₄N₂O₃
Molecular Weight:388.466
Hs Code.:

Synonyms:methyl (3β)-1-benzoyl-2,3-dihydroisolysergate

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Chemical Property of methyl (3β)-1-benzoyl-2,3-dihydroisolysergate

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Technology Process of methyl (3β)-1-benzoyl-2,3-dihydroisolysergate

There total 16 articles about methyl (3β)-1-benzoyl-2,3-dihydroisolysergate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 88636-20-8
(5aR,6aS,9R,10aR)-10a-Hydroxy-7-methyl-4,5,5a,6,6a,7,8,9,10,10a-decahydro-indolo[4,3-fg]quinoline-9-carboxylic acid methyl ester; hydrochloride

: 62592-69-2
methyl (3β)-1-benzoyl-2,3-dihydroisolysergate

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / P₂O₅, MeSO₃H / 3 h / Ambient temperature

2: pyridine / methanol / Ambient temperature

With pyridine; methanesulfonic acid; phosphorus pentoxide; In methanol;
DOI:10.1021/ja00318a044

Reference yield:

: 51867-06-2
1-benzoyl-1,2,2a,3-tetrahydrobenzindol-4-(5H)-one

: 62592-69-2
methyl (3β)-1-benzoyl-2,3-dihydroisolysergate

Guidance literature:: Multi-step reaction with 5 steps

1: 2.) triethylamine / 1.) benzene, reflux, 5 h.; 2.) benzene, reflux, 2 h.

3: 83 percent / trimethylamine N-oxide dihydrate / osmium tetraoxide / 2-methyl-propan-2-ol; pyridine; H₂O / 1 h / Heating

4: 1.) sodium metaperiodate; 2.) 4.0M chromium trioxide - sulphuric acid / 1.) methanol, water, room temp., 2 h.; 2.) aceton, water, 0 deg C, 1 h.

5: 85percent phosphoric acid, phosphoryl trichloride / pyridine

With chromium(VI) oxide; sodium periodate; trimethylamine-N-oxide; phosphoric acid; sulfuric acid; triethylamine; trichlorophosphate; osmium(VIII) oxide; In pyridine; water; tert-butyl alcohol;

Reference yield:

: 91421-20-4
N-(1-benzoyl-1,2,2a,3-tetrahydrobenzindol-4-yl)-N-methylfuran-3-carboxamide

: 62592-69-2
methyl (3β)-1-benzoyl-2,3-dihydroisolysergate

Guidance literature:: Multi-step reaction with 4 steps

2: 83 percent / trimethylamine N-oxide dihydrate / osmium tetraoxide / 2-methyl-propan-2-ol; pyridine; H₂O / 1 h / Heating

3: 1.) sodium metaperiodate; 2.) 4.0M chromium trioxide - sulphuric acid / 1.) methanol, water, room temp., 2 h.; 2.) aceton, water, 0 deg C, 1 h.

4: 85percent phosphoric acid, phosphoryl trichloride / pyridine

With chromium(VI) oxide; sodium periodate; trimethylamine-N-oxide; phosphoric acid; sulfuric acid; trichlorophosphate; osmium(VIII) oxide; In pyridine; water; tert-butyl alcohol;