4-[(10S)-dihydroartemisinin-10-oxy]benzaldehyde 4-(3,4-dimethylphenyl)thiosemicarbazone

Base Information

Chemical Name:4-[(10S)-dihydroartemisinin-10-oxy]benzaldehyde 4-(3,4-dimethylphenyl)thiosemicarbazone
CAS No.:1402318-31-3
Molecular Formula:C₃₁H₃₉N₃O₅S
Molecular Weight:565.734
Hs Code.:

Synonyms:4-[(10S)-dihydroartemisinin-10-oxy]benzaldehyde 4-(3,4-dimethylphenyl)thiosemicarbazone

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Chemical Property of 4-[(10S)-dihydroartemisinin-10-oxy]benzaldehyde 4-(3,4-dimethylphenyl)thiosemicarbazone

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Technology Process of 4-[(10S)-dihydroartemisinin-10-oxy]benzaldehyde 4-(3,4-dimethylphenyl)thiosemicarbazone

There total 7 articles about 4-[(10S)-dihydroartemisinin-10-oxy]benzaldehyde 4-(3,4-dimethylphenyl)thiosemicarbazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 32.7%

: 1287216-57-2
(10S)-10-(4-formylphenyl)dihydroartemisinin

: 6610-33-9
4-(3',4'-dimethylphenyl)-3-thiosemicarbazide

: 1402318-31-3
4-[(10S)-dihydroartemisinin-10-oxy]benzaldehyde 4-(3,4-dimethylphenyl)thiosemicarbazone

Guidance literature:: With acetic acid; In ethanol; at 20 ℃; for 2h;
DOI:10.1007/s12272-012-0902-4

Reference yield:

: 95-64-7
4-amino-o-xylene

: 1402318-31-3
4-[(10S)-dihydroartemisinin-10-oxy]benzaldehyde 4-(3,4-dimethylphenyl)thiosemicarbazone

Guidance literature:: Multi-step reaction with 4 steps

1: ammonium hydroxide / ethanol / 1 h / 20 °C

2: ethanol / 0.5 h / 20 °C

3: hydrazine hydrate / ethanol / 1 h / 20 °C

4: acetic acid / ethanol / 2 h / 20 °C

With ammonium hydroxide; hydrazine hydrate; acetic acid; In ethanol;
DOI:10.1007/s12272-012-0902-4

Reference yield:

: 63968-64-9
C₁₂H₁₃O₂(CH₃)3(O)(OO)

: 1402318-31-3
4-[(10S)-dihydroartemisinin-10-oxy]benzaldehyde 4-(3,4-dimethylphenyl)thiosemicarbazone

Guidance literature:: Multi-step reaction with 4 steps

1: sodium tetrahydroborate / methanol / 3.3 h / 0 - 5 °C

2: triethylamine / dichloromethane / 24 h / -5 - 0 °C

3: dichloromethane / 12 h / -5 - 0 °C

4: acetic acid / ethanol / 2 h / 20 °C

With sodium tetrahydroborate; acetic acid; triethylamine; In methanol; ethanol; dichloromethane;
DOI:10.1007/s12272-012-0902-4