(S)-6-benzyloxycarbonylamino-2-(2-oxooxazolidinesulfonylamino)hexanoic acid benzyl ester

Base Information

• Chemical Name: (S)-6-benzyloxycarbonylamino-2-(2-oxooxazolidinesulfonylamino)hexanoic acid benzyl ester
• CAS No.: 1032767-79-5
• Molecular Formula: C₂₄H₂₉N₃O₈S
• Molecular Weight: 519.576

Synonyms:(S)-6-benzyloxycarbonylamino-2-(2-oxooxazolidinesulfonylamino)hexanoic acid benzyl ester

Chemical Property of (S)-6-benzyloxycarbonylamino-2-(2-oxooxazolidinesulfonylamino)hexanoic acid benzyl ester

Chemical Property:

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Technology Process of (S)-6-benzyloxycarbonylamino-2-(2-oxooxazolidinesulfonylamino)hexanoic acid benzyl ester

There total 1 articles about (S)-6-benzyloxycarbonylamino-2-(2-oxooxazolidinesulfonylamino)hexanoic acid benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Ne-t-butoxycarbonyl-L-lysine benzyl ester hydrochloride (133170-57-7) + 2‐oxo‐1,3‐oxazolidine‐3‐sulfonyl chloride (710286-63-8) → (S)-6-benzyloxycarbonylamino-2-(2-oxooxazolidinesulfonylamino)hexanoic acid benzyl ester (1032767-79-5)

Guidance literature:

With triethylamine; In dichloromethane; at 10 - 20 ℃;

Reference yield:

(S)-6-benzyloxycarbonylamino-2-(2-oxooxazolidinesulfonylamino)hexanoic acid benzyl ester (1032767-79-5) + (S)-2-amino-3-cyclohexyl-N-((1R,2S,4R)-1,7,7-trimethyl-bicyclo[2.2.1]hept-2-yl)-propionamide trifluoroacetate → (S)-6-benzyloxycarbonylamino-2-{[(S)-2-cyclohexyl-1-((1R,2S,4R)-1,7,7-trimethylbicyclo[2.2.1]hept-2-ylcarbamoyl)ethylsulfamidyl]}hexanoic acid benzyl ester (1032767-83-1)

Guidance literature:

With triethylamine; In acetonitrile; for 20h; Reflux;

Reference yield:

(S)-6-benzyloxycarbonylamino-2-(2-oxooxazolidinesulfonylamino)hexanoic acid benzyl ester (1032767-79-5) + C13H26N2O*C2HF3O2 → C34H50N4O7S

Guidance literature:

With triethylamine; In acetonitrile; for 20h; Reflux;

DOI:10.1021/acs.jmedchem.6b01276

upstream raw materials:

Ne-t-butoxycarbonyl-L-lysine benzyl ester hydrochloride

2‐oxo‐1,3‐oxazolidine‐3‐sulfonyl chloride

Downstream raw materials:

(S)-6-benzyloxycarbonylamino-2-{[(S)-2-cyclohexyl-1-((1R,2S,4R)-1,7,7-trimethylbicyclo[2.2.1]hept-2-ylcarbamoyl)ethylsulfamidyl]}hexanoic acid benzyl ester

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