Technology Process of C44H60N8O17P2*ClH
There total 5 articles about C44H60N8O17P2*ClH which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
hydrogenchloride;
In
water;
at 60 ℃;
for 72h;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: potassium sulfite / acetonitrile / 48 h / 60 °C / Inert atmosphere
2: triethylamine; tetrakis(triphenylphosphine) palladium(0) / benzene / 60 °C
3: triethylamine; bis-triphenylphosphine-palladium(II) chloride / toluene / 12 h / 70 °C
4: hydrogenchloride / water / 72 h / 60 °C
With
hydrogenchloride; bis-triphenylphosphine-palladium(II) chloride; potassium sulfite; tetrakis(triphenylphosphine) palladium(0); triethylamine;
In
water; toluene; acetonitrile; benzene;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: triethylamine; tetrakis(triphenylphosphine) palladium(0) / benzene / 60 °C
2: triethylamine; bis-triphenylphosphine-palladium(II) chloride / toluene / 12 h / 70 °C
3: hydrogenchloride / water / 72 h / 60 °C
With
hydrogenchloride; bis-triphenylphosphine-palladium(II) chloride; tetrakis(triphenylphosphine) palladium(0); triethylamine;
In
water; toluene; benzene;