C₄₁H₅₂O₇

Base Information

Chemical Name:C₄₁H₅₂O₇
CAS No.:1264660-71-0
Molecular Formula:C₄₁H₅₂O₇
Molecular Weight:656.86
Hs Code.:

C<sub>41</sub>H<sub>52</sub>O<sub>7</sub>

Synonyms:C₄₁H₅₂O₇

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Chemical Property of C₄₁H₅₂O₇

Chemical Property:

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Technology Process of C₄₁H₅₂O₇

There total 14 articles about C₄₁H₅₂O₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₄₀H₄₉NO₆

: 917-54-4
methyllithium

: 1264660-71-0
C₄₁H₅₂O₇

Guidance literature:: C₄₀H₄₉NO₆; methyllithium; In diethyl ether; at -78 - 0 ℃;

With water; ammonium chloride; In diethyl ether;
DOI:10.1021/ol102925d

Reference yield:

: 1225339-83-2
C₂₇H₂₇O₇P

: 1264660-71-0
C₄₁H₅₂O₇

Guidance literature:: Multi-step reaction with 13 steps

1.1: 9-bora-bicyclo[3.3.1]nonane / tetrahydrofuran / 0 °C

1.2: 1 h / 50 °C

2.1: dimethylsulfide borane complex / tetrahydrofuran / 0 - 20 °C

2.2: 0 - 20 °C

3.1: diisobutylaluminium hydride / hexane; dichloromethane / 0 - 20 °C

3.2: 2.5 h

4.1: 1H-imidazole / N,N-dimethyl-formamide / 20 °C

5.1: tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide / dichloromethane / 19 h / 20 °C / Molecular sieve

6.1: zinc trifluoromethanesulfonate / tetrahydrofuran / 20 °C

7.1: sodium hydride / tetrahydrofuran; mineral oil / 2 h / 20 °C

7.2: 15 h

8.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 1 h / -78 °C

9.1: n-heptane; dichloromethane / -78 - 0 °C

10.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.5 h / 20 °C

11.1: 2,6-dimethylpyridine / dichloromethane / -78 °C

12.1: dimethyl sulfoxide / 3 h / 20 - 80 °C

13.1: diethyl ether / -78 - 0 °C

With 1H-imidazole; 2,6-dimethylpyridine; tetrapropylammonium perruthennate; dimethylsulfide borane complex; tetrabutyl ammonium fluoride; zinc trifluoromethanesulfonate; sodium hydride; diisobutylaluminium hydride; 4-methylmorpholine N-oxide; 9-bora-bicyclo[3.3.1]nonane; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; diethyl ether; hexane; n-heptane; dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide; mineral oil; 1.2: Suzuki-Miyaura coupling;
DOI:10.1021/ol102925d

Reference yield:

: 1225339-88-7
C₄₃H₆₈O₇Si₂

: 1264660-71-0
C₄₁H₅₂O₇

Guidance literature:: Multi-step reaction with 12 steps

1.1: dimethylsulfide borane complex / tetrahydrofuran / 0 - 20 °C

1.2: 0 - 20 °C

2.1: diisobutylaluminium hydride / hexane; dichloromethane / 0 - 20 °C

2.2: 2.5 h

3.1: 1H-imidazole / N,N-dimethyl-formamide / 20 °C

4.1: tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide / dichloromethane / 19 h / 20 °C / Molecular sieve

5.1: zinc trifluoromethanesulfonate / tetrahydrofuran / 20 °C

6.1: sodium hydride / tetrahydrofuran; mineral oil / 2 h / 20 °C

6.2: 15 h

7.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 1 h / -78 °C

8.1: n-heptane; dichloromethane / -78 - 0 °C

9.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.5 h / 20 °C

10.1: 2,6-dimethylpyridine / dichloromethane / -78 °C

11.1: dimethyl sulfoxide / 3 h / 20 - 80 °C

12.1: diethyl ether / -78 - 0 °C

With 1H-imidazole; 2,6-dimethylpyridine; tetrapropylammonium perruthennate; dimethylsulfide borane complex; tetrabutyl ammonium fluoride; zinc trifluoromethanesulfonate; sodium hydride; diisobutylaluminium hydride; 4-methylmorpholine N-oxide; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; diethyl ether; hexane; n-heptane; dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide; mineral oil;
DOI:10.1021/ol102925d