2-(4-Bromophenoxy)-N-((R)-2-{3-[methanesulfonyl(2-trimethylsilylethoxymethyl)amino]-4-(2-trimethylsilylethoxy-methoxy)phenyl}-2-triethylsilyloxyethyl)acetamide

Base Information

• Chemical Name: 2-(4-Bromophenoxy)-N-((R)-2-{3-[methanesulfonyl(2-trimethylsilylethoxymethyl)amino]-4-(2-trimethylsilylethoxy-methoxy)phenyl}-2-triethylsilyloxyethyl)acetamide
• CAS No.: 851336-90-8
• Molecular Formula: C₃₅H₆₁BrN₂O₈SSi₃
• Molecular Weight: 834.104

Synonyms:2-(4-Bromophenoxy)-N-((R)-2-{3-[methanesulfonyl(2-trimethylsilylethoxymethyl)amino]-4-(2-trimethylsilylethoxy-methoxy)phenyl}-2-triethylsilyloxyethyl)acetamide

Chemical Property of 2-(4-Bromophenoxy)-N-((R)-2-{3-[methanesulfonyl(2-trimethylsilylethoxymethyl)amino]-4-(2-trimethylsilylethoxy-methoxy)phenyl}-2-triethylsilyloxyethyl)acetamide

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Technology Process of 2-(4-Bromophenoxy)-N-((R)-2-{3-[methanesulfonyl(2-trimethylsilylethoxymethyl)amino]-4-(2-trimethylsilylethoxy-methoxy)phenyl}-2-triethylsilyloxyethyl)acetamide

There total 1 articles about 2-(4-Bromophenoxy)-N-((R)-2-{3-[methanesulfonyl(2-trimethylsilylethoxymethyl)amino]-4-(2-trimethylsilylethoxy-methoxy)phenyl}-2-triethylsilyloxyethyl)acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-(4-Bromophenoxy)-N-[(R)-2-(4-hydroxy-3-methanesulfonyl-aminophenyl)-2-triethylsilyloxyethyl]acetamide (851336-80-6) + (2-trimethylethylsilylethoxy)methyl chloride (76513-69-4) → 2-(4-Bromophenoxy)-N-((R)-2-{3-[methanesulfonyl(2-trimethylsilylethoxymethyl)amino]-4-(2-trimethylsilylethoxy-methoxy)phenyl}-2-triethylsilyloxyethyl)acetamide (851336-90-8)

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 0 - 20 ℃; for 12h;

Reference yield:

2-(4-Bromophenoxy)-N-((R)-2-{3-[methanesulfonyl(2-trimethylsilylethoxymethyl)amino]-4-(2-trimethylsilylethoxy-methoxy)phenyl}-2-triethylsilyloxyethyl)acetamide (851336-90-8) → 2-(4-bromophenoxy)-N-((R)-2-hydroxy-2-{3-[methanesulfonyl-(2-trimethylsilylethoxymethyl)amino]-4-(2-trimethylsilyl-ethoxymethoxy)phenyl}ethyl)acetamide (851336-99-7)

Guidance literature:

With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 20 ℃; for 14.5h;

upstream raw materials:

2-(4-Bromophenoxy)-N-[(R)-2-(4-hydroxy-3-methanesulfonyl-aminophenyl)-2-triethylsilyloxyethyl]acetamide

(2-trimethylethylsilylethoxy)methyl chloride

Downstream raw materials:

2-(4-bromophenoxy)-N-((R)-2-hydroxy-2-{3-[methanesulfonyl-(2-trimethylsilylethoxymethyl)amino]-4-(2-trimethylsilyl-ethoxymethoxy)phenyl}ethyl)acetamide

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