Technology Process of C23H26Cl2N6O4S
There total 8 articles about C23H26Cl2N6O4S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
sodium hydrogencarbonate;
In
tetrahydrofuran;
at 20 ℃;
for 36h;
- Guidance literature:
-
Multi-step reaction with 7 steps
1.1: caesium carbonate / N,N-dimethyl-formamide / 4 h
2.1: sodium bis(trimethylsilyl)amide / tetrahydrofuran; hexanes / -78 - -40 °C
2.2: -78 - -40 °C
2.3: -78 - 20 °C
3.1: hydrazinium monoacetate / ethanol / 16 h / 20 °C
4.1: sodium methylate / methanol / 5 h / 78 °C
5.1: trichlorophosphate / 3 h / 100 °C
6.1: oxalyl dichloride / dichloromethane; N,N-dimethyl-formamide / 3 h / 20 °C
6.2: 0.67 h / 20 °C / Cooling with ice
7.1: sodium hydrogencarbonate / tetrahydrofuran / 36 h / 20 °C
With
oxalyl dichloride; sodium bis(trimethylsilyl)amide; sodium methylate; hydrazinium monoacetate; sodium hydrogencarbonate; caesium carbonate; trichlorophosphate;
In
tetrahydrofuran; methanol; hexanes; ethanol; dichloromethane; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: sodium bis(trimethylsilyl)amide / tetrahydrofuran / 0.42 h / -78 - -20 °C / Inert atmosphere
1.2: 3.08 h / -78 - -45 °C
1.3: -78 - 20 °C
2.1: hydrazinium monoacetate / ethanol / 16 h / 20 °C
3.1: sodium methylate / methanol / 5 h / 78 °C
4.1: trichlorophosphate / 3 h / 100 °C
5.1: oxalyl dichloride / dichloromethane; N,N-dimethyl-formamide / 3 h / 20 °C
5.2: 0.67 h / 20 °C / Cooling with ice
6.1: sodium hydrogencarbonate / tetrahydrofuran / 36 h / 20 °C
With
oxalyl dichloride; sodium bis(trimethylsilyl)amide; sodium methylate; hydrazinium monoacetate; sodium hydrogencarbonate; trichlorophosphate;
In
tetrahydrofuran; methanol; ethanol; dichloromethane; N,N-dimethyl-formamide;