13α-acetoxymethyl-3-benzyloxy-14β-(prop-2-en-yl)-des-D-estra-1,3,5(10)-triene

Base Information

Chemical Name:13α-acetoxymethyl-3-benzyloxy-14β-(prop-2-en-yl)-des-D-estra-1,3,5(10)-triene
CAS No.:1620902-32-0
Molecular Formula:C₂₈H₃₄O₃
Molecular Weight:418.576
Hs Code.:

Synonyms:13α-acetoxymethyl-3-benzyloxy-14β-(prop-2-en-yl)-des-D-estra-1,3,5(10)-triene

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Chemical Property of 13α-acetoxymethyl-3-benzyloxy-14β-(prop-2-en-yl)-des-D-estra-1,3,5(10)-triene

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Technology Process of 13α-acetoxymethyl-3-benzyloxy-14β-(prop-2-en-yl)-des-D-estra-1,3,5(10)-triene

There total 2 articles about 13α-acetoxymethyl-3-benzyloxy-14β-(prop-2-en-yl)-des-D-estra-1,3,5(10)-triene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 108-24-7
acetic anhydride

: 313468-78-9
3-benzyloxy-13α-hydroxymethyl-14β-(prop-2-en-yl)-des-D-estra-1,3,5(10)-triene

: 1620902-32-0
13α-acetoxymethyl-3-benzyloxy-14β-(prop-2-en-yl)-des-D-estra-1,3,5(10)-triene

Guidance literature:: With silica gel; at 160 ℃; for 0.0833333h; Microwave irradiation;
DOI:10.1016/j.steroids.2014.05.015

Reference yield:

: 3-benzyloxy-14β-(prop-2-en-yl)-des-D-estra-1,3,5(10)-trien-13α-carbaldehyde

: 1620902-32-0
13α-acetoxymethyl-3-benzyloxy-14β-(prop-2-en-yl)-des-D-estra-1,3,5(10)-triene

Guidance literature:: Multi-step reaction with 2 steps

1: potassium borohydride / methanol; dichloromethane / 0.5 h / 20 °C / Cooling with ice

2: silica gel / 0.08 h / 160 °C / Microwave irradiation

With potassium borohydride; silica gel; In methanol; dichloromethane;
DOI:10.1016/j.steroids.2014.05.015