2,3-diphenyl-5-(3,4,5-tris(dodecyloxy)-1-benzyloxypropyl)-1,4-bis(hydroxymethyl)benzene

Base Information

Chemical Name:2,3-diphenyl-5-(3,4,5-tris(dodecyloxy)-1-benzyloxypropyl)-1,4-bis(hydroxymethyl)benzene
CAS No.:1376711-97-5
Molecular Formula:C₆₆H₁₀₂O₆
Molecular Weight:991.532
Hs Code.:

Synonyms:2,3-diphenyl-5-(3,4,5-tris(dodecyloxy)-1-benzyloxypropyl)-1,4-bis(hydroxymethyl)benzene

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Chemical Property of 2,3-diphenyl-5-(3,4,5-tris(dodecyloxy)-1-benzyloxypropyl)-1,4-bis(hydroxymethyl)benzene

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Technology Process of 2,3-diphenyl-5-(3,4,5-tris(dodecyloxy)-1-benzyloxypropyl)-1,4-bis(hydroxymethyl)benzene

There total 7 articles about 2,3-diphenyl-5-(3,4,5-tris(dodecyloxy)-1-benzyloxypropyl)-1,4-bis(hydroxymethyl)benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 1376711-96-4
diethyl 2,3-diphenyl-5-(3,4,5-tris(dodecyloxy)-1-benzyloxypropyl)terephthalate

: 1376711-97-5
2,3-diphenyl-5-(3,4,5-tris(dodecyloxy)-1-benzyloxypropyl)-1,4-bis(hydroxymethyl)benzene

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; at 0 ℃; for 12h; Inert atmosphere; Reflux;
DOI:10.1021/ma300640n

Reference yield:

: 1376711-95-3
3,4,5-tris(dodecyloxy)-1-benzyloxypent-4-yne

: 1376711-97-5
2,3-diphenyl-5-(3,4,5-tris(dodecyloxy)-1-benzyloxypropyl)-1,4-bis(hydroxymethyl)benzene

Guidance literature:: Multi-step reaction with 2 steps

1: toluene / 12 h / Reflux; Inert atmosphere

2: lithium aluminium tetrahydride / tetrahydrofuran / 12 h / 0 °C / Inert atmosphere; Reflux

With lithium aluminium tetrahydride; In tetrahydrofuran; toluene; 1: Diels-Alder reaction;
DOI:10.1021/ma300640n

Reference yield:

: 143-15-7
1-dodecylbromide

: 1376711-97-5
2,3-diphenyl-5-(3,4,5-tris(dodecyloxy)-1-benzyloxypropyl)-1,4-bis(hydroxymethyl)benzene

Guidance literature:: Multi-step reaction with 6 steps

1: potassium carbonate / acetonitrile

2: lithium aluminium tetrahydride / tetrahydrofuran

3: thionyl chloride / dichloromethane

4: tetrabutylammomium bromide; sodium hydride / tetrahydrofuran / 12 h / Inert atmosphere; Reflux

5: toluene / 12 h / Reflux; Inert atmosphere

6: lithium aluminium tetrahydride / tetrahydrofuran / 12 h / 0 °C / Inert atmosphere; Reflux

With lithium aluminium tetrahydride; thionyl chloride; tetrabutylammomium bromide; sodium hydride; potassium carbonate; In tetrahydrofuran; dichloromethane; toluene; acetonitrile; 5: Diels-Alder reaction;
DOI:10.1021/ma300640n