N,N-Diphenyl-N'-[3-((Z)-3-tributylstannanyl-propenyloxy)-prop-(E)-ylidene]-hydrazine

Base Information

Chemical Name:N,N-Diphenyl-N'-[3-((Z)-3-tributylstannanyl-propenyloxy)-prop-(E)-ylidene]-hydrazine
CAS No.:234087-04-8
Molecular Formula:C₃₀H₄₆N₂OSn
Molecular Weight:569.418
Hs Code.:

Synonyms:N,N-Diphenyl-N'-[3-((Z)-3-tributylstannanyl-propenyloxy)-prop-(E)-ylidene]-hydrazine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N,N-Diphenyl-N'-[3-((Z)-3-tributylstannanyl-propenyloxy)-prop-(E)-ylidene]-hydrazine

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Technology Process of N,N-Diphenyl-N'-[3-((Z)-3-tributylstannanyl-propenyloxy)-prop-(E)-ylidene]-hydrazine

There total 1 articles about N,N-Diphenyl-N'-[3-((Z)-3-tributylstannanyl-propenyloxy)-prop-(E)-ylidene]-hydrazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 530-47-2,29666-92-0
N,N-diphenylhydrazine hydrochloride

: 3-((Z)-3-Tributylstannanyl-propenyloxy)-propionaldehyde

: 234087-04-8
N,N-Diphenyl-N'-[3-((Z)-3-tributylstannanyl-propenyloxy)-prop-(E)-ylidene]-hydrazine

Guidance literature:: With triethylamine; In dichloromethane; room temp.;
DOI:10.1039/CC9960000841

Reference yield: 82.0%

: 234087-04-8
N,N-Diphenyl-N'-[3-((Z)-3-tributylstannanyl-propenyloxy)-prop-(E)-ylidene]-hydrazine

: N,N-Diphenyl-N'-((2S,3R)-2-vinyl-tetrahydro-furan-3-yl)-hydrazine

Guidance literature:: With titanium(IV) dichlorodiisopropylate; In dichloromethane; at -78 ℃;
DOI:10.1039/CC9960000841

Reference yield:

: 234087-04-8
N,N-Diphenyl-N'-[3-((Z)-3-tributylstannanyl-propenyloxy)-prop-(E)-ylidene]-hydrazine

: 3-(N-benzoylamino)-2-vinyltetrahydrofuran

Guidance literature:: Multi-step reaction with 3 steps

1: 82 percent / TiCl₂(O-i-Pr)2 / CH₂Cl₂ / -78 °C

2: 82 percent / BuLi / tetrahydrofuran / 1.) -78 deg C, 2.) -78 deg C to r.t.

3: 45 percent / SmI₂ / tetrahydrofuran; hexamethylphosphoric acid triamide / Ambient temperature

With n-butyllithium; samarium diiodide; titanium(IV) dichlorodiisopropylate; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; dichloromethane;
DOI:10.1039/CC9960000841