Technology Process of C22H22(2)HNO8
There total 7 articles about C22H22(2)HNO8 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
triphenylphosphine; diethylazodicarboxylate;
In
tetrahydrofuran;
at 20 ℃;
for 4h;
DOI:10.1021/ja076604l
- Guidance literature:
-
Multi-step reaction with 6 steps
1: sodium tetrahydroborate / methanol
2: sodium hydride / N,N-dimethyl-formamide
3: acetic acid
4: sodium periodate; silica gel / dichloromethane; water
5: monodeuterioisoborneol; n-butyl magnesium bromide / tetrahydrofuran
6: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran
With
n-butyl magnesium bromide; sodium tetrahydroborate; sodium periodate; monodeuterioisoborneol; di-isopropyl azodicarboxylate; silica gel; sodium hydride; acetic acid; triphenylphosphine;
In
tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1021/jacs.5b03576
- Guidance literature:
-
Multi-step reaction with 5 steps
1: sodium hydride / N,N-dimethyl-formamide
2: acetic acid
3: sodium periodate; silica gel / dichloromethane; water
4: monodeuterioisoborneol; n-butyl magnesium bromide / tetrahydrofuran
5: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran
With
n-butyl magnesium bromide; sodium periodate; monodeuterioisoborneol; di-isopropyl azodicarboxylate; silica gel; sodium hydride; acetic acid; triphenylphosphine;
In
tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1021/jacs.5b03576
