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Technology Process of (1R,2R,3S,8S,10S,11S,13R)-10-(benzyloxy)-15,15-dimethyl-12,14,16-trioxatetracyclo<11.3.0.02,11.03,8>hexadecane-4,6-dione

(1R,2R,3S,8S,10S,11S,13R)-10-(benzyloxy)-15,15-dimethyl-12,14,16-trioxatetracyclo<11.3.0.02,11.03,8>hexadecane-4,6-dione

Base Information
  • Chemical Name:(1R,2R,3S,8S,10S,11S,13R)-10-(benzyloxy)-15,15-dimethyl-12,14,16-trioxatetracyclo<11.3.0.02,11.03,8>hexadecane-4,6-dione
  • CAS No.:142133-31-1
  • Molecular Formula:C22H26O6
  • Molecular Weight:386.445
  • Hs Code.:
(1R,2R,3S,8S,10S,11S,13R)-10-(benzyloxy)-15,15-dimethyl-12,14,16-trioxatetracyclo<11.3.0.0<sup>2,11</sup>.0<sup>3,8</sup>>hexadecane-4,6-dione

Synonyms:(1R,2R,3S,8S,10S,11S,13R)-10-(benzyloxy)-15,15-dimethyl-12,14,16-trioxatetracyclo<11.3.0.02,11.03,8>hexadecane-4,6-dione

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Chemical Property of (1R,2R,3S,8S,10S,11S,13R)-10-(benzyloxy)-15,15-dimethyl-12,14,16-trioxatetracyclo<11.3.0.02,11.03,8>hexadecane-4,6-dione
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Technology Process of (1R,2R,3S,8S,10S,11S,13R)-10-(benzyloxy)-15,15-dimethyl-12,14,16-trioxatetracyclo<11.3.0.02,11.03,8>hexadecane-4,6-dione

There total 1 articles about (1R,2R,3S,8S,10S,11S,13R)-10-(benzyloxy)-15,15-dimethyl-12,14,16-trioxatetracyclo<11.3.0.02,11.03,8>hexadecane-4,6-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 15.0%

(1R,3S,4R,5R)-3-<(1S,3E)-1-(benzyloxy)-4-(ethoxycarbonyl)-3-butenyl>-4-(2-oxopropyl)-7,7-dimethyl-2,6,8-trioxabicyclo<3.3.0>octane
142133-20-8

(1R,3S,4R,5R)-3-<(1S,3E)-1-(benzyloxy)-4-(ethoxycarbonyl)-3-butenyl>-4-(2-oxopropyl)-7,7-dimethyl-2,6,8-trioxabicyclo<3.3.0>octane

(1R,2R,3S,8R,10S,11S,13R)-10-(benzyloxy)-6-hydroxy-15,15-dimethyl-12,14,16-trioxatetracyclo<11.3.0.0<sup>2,11</sup>.0<sup>3,8</sup>>hexadec-5-en-4-one
142133-30-0

(1R,2R,3S,8R,10S,11S,13R)-10-(benzyloxy)-6-hydroxy-15,15-dimethyl-12,14,16-trioxatetracyclo<11.3.0.02,11.03,8>hexadec-5-en-4-one

(1R,2R,3S,8S,10S,11S,13R)-10-(benzyloxy)-15,15-dimethyl-12,14,16-trioxatetracyclo<11.3.0.0<sup>2,11</sup>.0<sup>3,8</sup>>hexadecane-4,6-dione
142133-31-1

(1R,2R,3S,8S,10S,11S,13R)-10-(benzyloxy)-15,15-dimethyl-12,14,16-trioxatetracyclo<11.3.0.02,11.03,8>hexadecane-4,6-dione

Guidance literature:
With sodium hydride; In N,N-dimethyl-formamide; at 0 ℃; for 1.5h;
DOI:10.1021/jo00042a034
upstream raw materials:

(1R,3S,4R,5R)-3-<(1S,3E)-1-(benzyloxy)-4-(ethoxycarbonyl)-3-butenyl>-4-(2-oxopropyl)-7,7-dimethyl-2,6,8-trioxabicyclo<3.3.0>octane

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