4-(4-(bis(4-(hexyloxy)phenyl)amino)styryl)-2,5-bis(hexyloxy)benzaldehyde

Base Information

Chemical Name:4-(4-(bis(4-(hexyloxy)phenyl)amino)styryl)-2,5-bis(hexyloxy)benzaldehyde
CAS No.:1360744-00-8
Molecular Formula:C₅₁H₆₉NO₅
Molecular Weight:776.113
Hs Code.:

Synonyms:4-(4-(bis(4-(hexyloxy)phenyl)amino)styryl)-2,5-bis(hexyloxy)benzaldehyde

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Chemical Property of 4-(4-(bis(4-(hexyloxy)phenyl)amino)styryl)-2,5-bis(hexyloxy)benzaldehyde

Chemical Property:

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Technology Process of 4-(4-(bis(4-(hexyloxy)phenyl)amino)styryl)-2,5-bis(hexyloxy)benzaldehyde

There total 9 articles about 4-(4-(bis(4-(hexyloxy)phenyl)amino)styryl)-2,5-bis(hexyloxy)benzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 1360743-98-1
4-(hexyloxy)-N-(4-(hexyloxy)phenyl)-N-(4-vinylphenyl)aniline

: 2,5-bis(hexyloxy)-4-iodobenzaldehyde

: 1360744-00-8
4-(4-(bis(4-(hexyloxy)phenyl)amino)styryl)-2,5-bis(hexyloxy)benzaldehyde

Guidance literature:: With trans-di(μ-acetato)bis[o-(di-o-tolylphosphino)benzyl]dipalladium(II); trimethylamine; In N,N-dimethyl acetamide; at 80 ℃; for 72h; Inert atmosphere;
DOI:10.1016/j.dyepig.2011.10.014

Reference yield:

: 111-25-1
1-bromo-hexane

: 1360744-00-8
4-(4-(bis(4-(hexyloxy)phenyl)amino)styryl)-2,5-bis(hexyloxy)benzaldehyde

Guidance literature:: Multi-step reaction with 4 steps

1.1: potassium hydroxide / ethanol / 24 h / Reflux

2.1: iodine; periodic acid / methanol / 4 h / 70 °C

3.1: n-butyllithium / diethyl ether; hexane / 1.33 h / -10 - -5 °C

3.2: 6 h / 20 °C

4.1: trans-di(μ-acetato)bis[o-(di-o-tolylphosphino)benzyl]dipalladium(II); trimethylamine / N,N-dimethyl acetamide / 72 h / 80 °C / Inert atmosphere

With n-butyllithium; trans-di(μ-acetato)bis[o-(di-o-tolylphosphino)benzyl]dipalladium(II); iodine; periodic acid; potassium hydroxide; trimethylamine; In methanol; diethyl ether; ethanol; hexane; N,N-dimethyl acetamide; 1.1: Williamson synthesis / 4.1: Heck reaction;
DOI:10.1016/j.dyepig.2011.10.014

Reference yield:

: 1146433-75-1
4-(hexyloxy)-N-(4-(hexyloxy)phenyl)-N-phenylaniline

: 1360744-00-8
4-(4-(bis(4-(hexyloxy)phenyl)amino)styryl)-2,5-bis(hexyloxy)benzaldehyde

Guidance literature:: Multi-step reaction with 3 steps

1: trichlorophosphate / 48 h / 0 - 20 °C

2: potassium tert-butylate / tetrahydrofuran / 8 h / 20 °C / Inert atmosphere

3: trans-di(μ-acetato)bis[o-(di-o-tolylphosphino)benzyl]dipalladium(II); trimethylamine / N,N-dimethyl acetamide / 72 h / 80 °C / Inert atmosphere

With trans-di(μ-acetato)bis[o-(di-o-tolylphosphino)benzyl]dipalladium(II); potassium tert-butylate; trimethylamine; trichlorophosphate; In tetrahydrofuran; N,N-dimethyl acetamide; 1: Vilsmeier-Haack reaction / 3: Heck reaction;
DOI:10.1016/j.dyepig.2011.10.014