Phenylglycyl FP-12

Base Information

Chemical Name:Phenylglycyl FP-12
CAS No.:139953-98-3
Molecular Formula:C20H24O2
Molecular Weight:296.4034
Hs Code.:
DSSTox Substance ID:DTXSID701030663
Nikkaji Number:J460.227G

Synonyms:Phenylglycyl FP-12;Phenylglycyl fecapentaene-12;CCRIS 4373;(all-E)-alpha-((1,3,5,7,9-Dodecapentadienyloxy)methyl)benzenemethanol;2'-(1,3,5,7,9-Dodecapentaenyloxy)-1'-phenylethanol;139953-98-3;2'-(1,3,5,7,9-Dodecapentaenyloxy)-1'-phenyl ethanol;Benzenemethanol, alpha-((1,3,5,7,9-dodecapentadienyloxy)methyl)-, (all-E)-;DTXSID701030663;LS-30738;2-(1,3,5,7,9-Dodecapentenyloxy)-1-phenylethanol

Suppliers and Price of Phenylglycyl FP-12

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of Phenylglycyl FP-12

Chemical Property:

Vapor Pressure:1.75E-09mmHg at 25°C
Boiling Point:466°Cat760mmHg
Flash Point:205.7°C
Density:1.011g/cm³
XLogP3:4.9
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:9
Exact Mass:296.177630004
Heavy Atom Count:22
Complexity:396

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCC=CC=CC=CC=CC=COCC(C1=CC=CC=C1)O
Isomeric SMILES:CC/C=C/C=C/C=C/C=C/C=C/OCC(C1=CC=CC=C1)O

Technology Process of Phenylglycyl FP-12

There total 20 articles about Phenylglycyl FP-12 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2'-(1E/Z-dodecaenyloxy)-1'-phenylethanol

: 139953-98-3
2-[((1Z,3E,5E,7E,9E)-Dodeca-1,3,5,7,9-pentaenyl)oxy]-1-phenyl-ethanol

Guidance literature:: Multi-step reaction with 8 steps

1: 35 percent / H₂O / 3 h

2: 96 percent / imidazole / dimethylformamide / Ambient temperature

3: 92 percent / p-TsOH*H₂O / CH₂Cl₂ / Ambient temperature

4: 84 percent / Bu₄NF*3H₂O / tetrahydrofuran / 0 °C

5: 1.) NaH / 1.) THF, 40 min, 50 deg C, 2.) THF, -10 deg C, 15 min and 80 deg C

6: 87 percent / 20percent H₂SO₄ / methanol / 1 h / Ambient temperature

7: 92 percent / imidazole / dimethylformamide / 1 h / Ambient temperature

8: 2.) Bu₄NF*3H₂O

With 1H-imidazole; sulfuric acid; tetrabutyl ammonium fluoride; sodium hydride; toluene-4-sulfonic acid; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4020(01)89330-3

Reference yield:

: 2'-(1E/Z-dodecaenyloxy)-1'-phenylethanol

: 139953-98-3
2-[((1E,3E,5E,7E,9E)-Dodeca-1,3,5,7,9-pentaenyl)oxy]-1-phenyl-ethanol

Guidance literature:: Multi-step reaction with 8 steps

1: 35 percent / H₂O / 3 h

2: 96 percent / imidazole / dimethylformamide / Ambient temperature

3: 92 percent / p-TsOH*H₂O / CH₂Cl₂ / Ambient temperature

4: 84 percent / Bu₄NF*3H₂O / tetrahydrofuran / 0 °C

5: 1.) NaH / 1.) THF, 40 min, 50 deg C, 2.) THF, -10 deg C, 15 min and 80 deg C

6: 87 percent / 20percent H₂SO₄ / methanol / 1 h / Ambient temperature

7: 92 percent / imidazole / dimethylformamide / 1 h / Ambient temperature

8: 2.) Bu₄NF*3H₂O

With 1H-imidazole; sulfuric acid; tetrabutyl ammonium fluoride; sodium hydride; toluene-4-sulfonic acid; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4020(01)89330-3

Reference yield:

: 139953-98-3
2'-(1E/Z,3E,5E,7E,9E-dodecapentaenyloxy)-1'-phenylethanol

: 139953-98-3
2-[((1Z,3E,5E,7E,9E)-Dodeca-1,3,5,7,9-pentaenyl)oxy]-1-phenyl-ethanol

Guidance literature:: Multi-step reaction with 8 steps

1: 42 percent / H₂O / 4 h

2: 96 percent / imidazole / dimethylformamide / Ambient temperature

3: 92 percent / p-TsOH*H₂O / CH₂Cl₂ / Ambient temperature

4: 84 percent / Bu₄NF*3H₂O / tetrahydrofuran / 0 °C

5: 1.) NaH / 1.) THF, 40 min, 50 deg C, 2.) THF, -10 deg C, 15 min and 80 deg C

6: 87 percent / 20percent H₂SO₄ / methanol / 1 h / Ambient temperature

7: 92 percent / imidazole / dimethylformamide / 1 h / Ambient temperature

8: 2.) Bu₄NF*3H₂O

With 1H-imidazole; sulfuric acid; tetrabutyl ammonium fluoride; sodium hydride; toluene-4-sulfonic acid; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4020(01)89330-3