Technology Process of C26H40O7Si
There total 7 articles about C26H40O7Si which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
methanesulfonamide; AD-mix β;
In
water; tert-butyl alcohol;
at 0 ℃;
for 40h;
DOI:10.1002/anie.201203935
- Guidance literature:
-
Multi-step reaction with 5 steps
1: toluene-4-sulfonic acid / methanol / 3 h / 20 °C
2: pyridine / dichloromethane / 1.5 h / 0 °C
3: dmap / 2.5 h / 0 - 20 °C
4: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / tetrahydrofuran / 2.75 h / 20 °C
5: AD-mix β; methanesulfonamide / water; tert-butyl alcohol / 40 h / 0 °C
With
pyridine; dmap; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; methanesulfonamide; AD-mix β; toluene-4-sulfonic acid; triethylamine;
In
tetrahydrofuran; methanol; dichloromethane; water; tert-butyl alcohol;
4: Sonogashira coupling / 5: Sharpless dihydroxylation;
DOI:10.1002/anie.201203935
- Guidance literature:
-
Multi-step reaction with 4 steps
1: pyridine / dichloromethane / 1.5 h / 0 °C
2: dmap / 2.5 h / 0 - 20 °C
3: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / tetrahydrofuran / 2.75 h / 20 °C
4: AD-mix β; methanesulfonamide / water; tert-butyl alcohol / 40 h / 0 °C
With
pyridine; dmap; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; methanesulfonamide; AD-mix β; triethylamine;
In
tetrahydrofuran; dichloromethane; water; tert-butyl alcohol;
3: Sonogashira coupling / 4: Sharpless dihydroxylation;
DOI:10.1002/anie.201203935
