Technology Process of C24H21BrO4
There total 4 articles about C24H21BrO4 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
acetic acid; tetramethylammonium triacetoxyborohydride;
In
acetonitrile;
at 20 ℃;
for 3h;
Inert atmosphere;
DOI:10.1021/jm101318b
- Guidance literature:
-
Multi-step reaction with 4 steps
1: methanol; dichloromethane / 15 h / 0 °C / Irradiation; Inert atmosphere
2: sodium methylate / methanol / 0.33 h / 60 °C / Inert atmosphere
3: water; lithium chloride / dimethyl sulfoxide / 12 h / 100 °C
4: acetic acid; tetramethylammonium triacetoxyborohydride / acetonitrile / 3 h / 20 °C / Inert atmosphere
With
water; sodium methylate; acetic acid; lithium chloride; tetramethylammonium triacetoxyborohydride;
In
methanol; dichloromethane; dimethyl sulfoxide; acetonitrile;
DOI:10.1021/jm101318b
- Guidance literature:
-
Multi-step reaction with 4 steps
1: methanol; dichloromethane / 15 h / 0 °C / Irradiation; Inert atmosphere
2: sodium methylate / methanol / 0.33 h / 60 °C / Inert atmosphere
3: water; lithium chloride / dimethyl sulfoxide / 12 h / 100 °C
4: acetic acid; tetramethylammonium triacetoxyborohydride / acetonitrile / 3 h / 20 °C / Inert atmosphere
With
water; sodium methylate; acetic acid; lithium chloride; tetramethylammonium triacetoxyborohydride;
In
methanol; dichloromethane; dimethyl sulfoxide; acetonitrile;
DOI:10.1021/jm101318b
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