methyl 4-<(4-acetyl-3-hydroxy-2-prop-2-enylphenoxy)methyl>-3-methoxybenzoate

Base Information

Chemical Name:methyl 4-<(4-acetyl-3-hydroxy-2-prop-2-enylphenoxy)methyl>-3-methoxybenzoate
CAS No.:118683-90-2
Molecular Formula:C₂₁H₂₂O₆
Molecular Weight:370.402
Hs Code.:

Synonyms:methyl 4-<(4-acetyl-3-hydroxy-2-prop-2-enylphenoxy)methyl>-3-methoxybenzoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl 4-<(4-acetyl-3-hydroxy-2-prop-2-enylphenoxy)methyl>-3-methoxybenzoate

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Technology Process of methyl 4-<(4-acetyl-3-hydroxy-2-prop-2-enylphenoxy)methyl>-3-methoxybenzoate

There total 1 articles about methyl 4-<(4-acetyl-3-hydroxy-2-prop-2-enylphenoxy)methyl>-3-methoxybenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 38987-00-7
2,4-dihydroxy-3-allylacetophenone

: 70264-94-7
methyl 4-(bromomethyl)-3-methoxybenzoate

: 118683-90-2
methyl 4-<(4-acetyl-3-hydroxy-2-prop-2-enylphenoxy)methyl>-3-methoxybenzoate

Guidance literature:: With potassium carbonate; In acetone; for 48h; Heating;
DOI:10.1021/jm00124a014

Reference yield: 84.0%

: 98-59-9
p-toluenesulfonyl chloride

: 118683-90-2
methyl 4-<(4-acetyl-3-hydroxy-2-prop-2-enylphenoxy)methyl>-3-methoxybenzoate

: 118683-91-3
methyl 4-<<4-acetyl-3-<<(4-methylphenyl)sulfonyl>oxy>-2-prop-2-enylphenoxy>methyl>-3-methoxybenzoate

Guidance literature:: With potassium carbonate; In acetone; for 12h; Heating;
DOI:10.1021/jm00124a014

Reference yield:

: 118683-90-2
methyl 4-<(4-acetyl-3-hydroxy-2-prop-2-enylphenoxy)methyl>-3-methoxybenzoate

: 118683-10-6
4-[4-Acetyl-3-hydroxy-2-(4-oxo-pentyl)-phenoxymethyl]-3-methoxy-benzoic acid

Guidance literature:: Multi-step reaction with 5 steps

1: 84 percent / K₂CO₃ / acetone / 12 h / Heating

2: 1) O₃, 2) Me₂S / 1) CH₂Cl₂, MeOH, -78 deg C, 30 min, 2) rt, 30 min

3: 65 percent / tetrahydrofuran / 16 h / Heating

4: 70 percent / H₂ / PtO₂ (prereduced) / ethyl acetate / 3 h / 760 Torr / Ambient temperature

5: LiOH*H₂O / tetrahydrofuran; methanol; H₂O / Ambient temperature

With lithium hydroxide; dimethylsulfide; hydrogen; potassium carbonate; ozone; platinum(IV) oxide; In tetrahydrofuran; methanol; water; ethyl acetate; acetone;
DOI:10.1021/jm00124a014