[1-[4-(aminosulfonyl)-2-fluorophenyl]-5-(2,5-dimethylbenzyl)-1H-1,2,4-triazol-3-yl]methyl N-(tert-butoxycarbonyl)-L-valinate

Base Information

Chemical Name:[1-[4-(aminosulfonyl)-2-fluorophenyl]-5-(2,5-dimethylbenzyl)-1H-1,2,4-triazol-3-yl]methyl N-(tert-butoxycarbonyl)-L-valinate
CAS No.:1034471-91-4
Molecular Formula:C₂₈H₃₆FN₅O₆S
Molecular Weight:589.688
Hs Code.:

Synonyms:[1-[4-(aminosulfonyl)-2-fluorophenyl]-5-(2,5-dimethylbenzyl)-1H-1,2,4-triazol-3-yl]methyl N-(tert-butoxycarbonyl)-L-valinate

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Chemical Property of [1-[4-(aminosulfonyl)-2-fluorophenyl]-5-(2,5-dimethylbenzyl)-1H-1,2,4-triazol-3-yl]methyl N-(tert-butoxycarbonyl)-L-valinate

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Technology Process of [1-[4-(aminosulfonyl)-2-fluorophenyl]-5-(2,5-dimethylbenzyl)-1H-1,2,4-triazol-3-yl]methyl N-(tert-butoxycarbonyl)-L-valinate

There total 1 articles about [1-[4-(aminosulfonyl)-2-fluorophenyl]-5-(2,5-dimethylbenzyl)-1H-1,2,4-triazol-3-yl]methyl N-(tert-butoxycarbonyl)-L-valinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 13734-41-3
t-Boc-L-valine

: 1034471-82-3
4-[3-(chloromethyl)-5-(2,5-dimethylbenzyl)-1H-1,2,4-triazol-1-yl]-3-fluorobenzenesulfonamide

: 1034471-91-4
[1-[4-(aminosulfonyl)-2-fluorophenyl]-5-(2,5-dimethylbenzyl)-1H-1,2,4-triazol-3-yl]methyl N-(tert-butoxycarbonyl)-L-valinate

Guidance literature:: With potassium carbonate; potassium iodide; In N,N-dimethyl-formamide; at 60 ℃; for 16h;

Reference yield: 65.0%

: 1034471-91-4
[1-[4-(aminosulfonyl)-2-fluorophenyl]-5-(2,5-dimethylbenzyl)-1H-1,2,4-triazol-3-yl]methyl N-(tert-butoxycarbonyl)-L-valinate

: 1006912-84-0
[1-[4-(aminosulfonyl)-2-fluorophenyl]-5-(2,5-dimethylbenzyl)-1H-1,2,4-triazol-3-yl]methyl L-valinate

Guidance literature:: [1-[4-(aminosulfonyl)-2-fluorophenyl]-5-(2,5-dimethylbenzyl)-1H-1,2,4-triazol-3-yl]methyl N-(tert-butoxycarbonyl)-L-valinate; With trifluoroacetic acid; In dichloromethane; for 4h;

With water; sodium hydrogencarbonate; In dichloromethane;