<26,27-2H6>desmosteryl benzoate

Base Information

Chemical Name:<26,27-2H6>desmosteryl benzoate
CAS No.:88247-71-6
Molecular Formula:C₃₄H₄₈O₂
Molecular Weight:494.706
Hs Code.:

Synonyms:<26,27-2H6>desmosteryl benzoate

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Chemical Property of <26,27-2H6>desmosteryl benzoate

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Technology Process of <26,27-2H6>desmosteryl benzoate

There total 4 articles about <26,27-2H6>desmosteryl benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 75303-40-1
24-phenylsulphonylchol-5-en-3β-ol 3-tetrahydropyranyl ether

: 88247-71-6
<26,27-2H6>desmosteryl benzoate

Guidance literature:: Multi-step reaction with 4 steps

1: 81 percent / 1.) litium di-isopropylamide / tetrahydrofuran / 0.5 h / 0 °C

2: 48 percent / sodium amalgam / tetrahydrofuran; methanol / 4 h / Ambient temperature

3: hydrochloric acid / tetrahydrofuran; methanol / 17 h / Ambient temperature

4: 2.14 g / pyridine / 20 h

With pyridine; hydrogenchloride; sodium amalgam; lithium diisopropyl amide; In tetrahydrofuran; methanol;
DOI:10.1039/P19830002563

Reference yield:

: 88255-62-3
<26,27-2H6>cholesta-5,24-dien-3β-ol 3-tetrahydropyran-2-yl ether

: 88247-71-6
<26,27-2H6>desmosteryl benzoate

Guidance literature:: Multi-step reaction with 2 steps

1: hydrochloric acid / tetrahydrofuran; methanol / 17 h / Ambient temperature

2: 2.14 g / pyridine / 20 h

With pyridine; hydrogenchloride; In tetrahydrofuran; methanol;
DOI:10.1039/P19830002563

Reference yield:

: 88247-66-9
(24R,S)-24-phenylsulphonyl<26,27-2H6>cholest-5-ene-3β,25-diol 3-tetrahydropyran-2-yl ether

: 88247-71-6
<26,27-2H6>desmosteryl benzoate

Guidance literature:: Multi-step reaction with 3 steps

1: 48 percent / sodium amalgam / tetrahydrofuran; methanol / 4 h / Ambient temperature

2: hydrochloric acid / tetrahydrofuran; methanol / 17 h / Ambient temperature

3: 2.14 g / pyridine / 20 h

With pyridine; hydrogenchloride; sodium amalgam; In tetrahydrofuran; methanol;
DOI:10.1039/P19830002563