N-{3-[(N,N-dimethylaminophenyl)-4'-diazenyl]phenylacetyl}-N-tert-butyloxycarbonylalanine methyl ester

Base Information

Chemical Name:N-{3-[(N,N-dimethylaminophenyl)-4'-diazenyl]phenylacetyl}-N-tert-butyloxycarbonylalanine methyl ester
CAS No.:713521-03-0
Molecular Formula:C₂₅H₃₂N₄O₅
Molecular Weight:468.553
Hs Code.:

Synonyms:N-{3-[(N,N-dimethylaminophenyl)-4'-diazenyl]phenylacetyl}-N-tert-butyloxycarbonylalanine methyl ester

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Chemical Property of N-{3-[(N,N-dimethylaminophenyl)-4'-diazenyl]phenylacetyl}-N-tert-butyloxycarbonylalanine methyl ester

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Technology Process of N-{3-[(N,N-dimethylaminophenyl)-4'-diazenyl]phenylacetyl}-N-tert-butyloxycarbonylalanine methyl ester

There total 2 articles about N-{3-[(N,N-dimethylaminophenyl)-4'-diazenyl]phenylacetyl}-N-tert-butyloxycarbonylalanine methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

: 24424-99-5
di-tert-butyl dicarbonate

: 661464-06-8
N-{3-[(N,N-dimethylaminophenyl)-4'-diazenyl]phenylacetyl}alanine methyl ester

: 713521-03-0
N-{3-[(N,N-dimethylaminophenyl)-4'-diazenyl]phenylacetyl}-N-tert-butyloxycarbonylalanine methyl ester

Guidance literature:: With dmap; In acetonitrile; at 20 ℃; for 48h;
DOI:10.1002/ejoc.200300692

Reference yield:

: 386207-00-7
3-[(N,N-dimethylaminophenyl)-4'-diazenyl]phenylacetic acid

: 713521-03-0
N-{3-[(N,N-dimethylaminophenyl)-4'-diazenyl]phenylacetyl}-N-tert-butyloxycarbonylalanine methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 71 percent / DCC; HOBt / dimethylformamide

2: 48 percent / DMAP / acetonitrile / 48 h / 20 °C

With dmap; benzotriazol-1-ol; dicyclohexyl-carbodiimide; In N,N-dimethyl-formamide; acetonitrile;
DOI:10.1002/ejoc.200300692