C₄₈H₇₁BrO₇Si₂

Base Information

Chemical Name:C₄₈H₇₁BrO₇Si₂
CAS No.:1388153-00-1
Molecular Formula:C₄₈H₇₁BrO₇Si₂
Molecular Weight:896.163
Hs Code.:

C<sub>48</sub>H<sub>71</sub>BrO<sub>7</sub>Si<sub>2</sub>

Synonyms:C₄₈H₇₁BrO₇Si₂

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Chemical Property of C₄₈H₇₁BrO₇Si₂

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Technology Process of C₄₈H₇₁BrO₇Si₂

There total 28 articles about C₄₈H₇₁BrO₇Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 1388152-99-5
C₄₈H₇₂O₇Si₂

: 1388153-00-1
C₄₈H₇₁BrO₇Si₂

Guidance literature:: With N-Bromosuccinimide; In acetonitrile; at 0 - 20 ℃; for 1h; stereoselective reaction;
DOI:10.1021/ja305864z

Reference yield:

: 1388153-33-0
C₃₄H₄₃NO₅Si

: 1388153-00-1
C₄₈H₇₁BrO₇Si₂

Guidance literature:: Multi-step reaction with 7 steps

1.1: sodium tetrahydroborate / tetrahydrofuran; water / 5 h / 0 - 20 °C

2.1: pyridinium p-toluenesulfonate / dichloromethane / 2 h / 20 °C

3.1: diisobutylaluminium hydride / hexane; dichloromethane / 2.5 h / -78 - -40 °C / Inert atmosphere

4.1: 1H-imidazole; iodine; triphenylphosphine / tetrahydrofuran / 0.5 h / 20 °C

5.1: tert.-butyl lithium; 9-methoxy-9-BBN / diethyl ether; hexane; pentane / 1.08 h / -78 - 20 °C / Inert atmosphere

5.2: 2 h / 50 °C / Inert atmosphere

6.1: Allyl ether; 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane / 1 h / 0 - 20 °C / pH 7 / aq. phosphate buffer

7.1: N-Bromosuccinimide / acetonitrile / 1 h / 0 - 20 °C

With 1H-imidazole; sodium tetrahydroborate; N-Bromosuccinimide; Allyl ether; iodine; tert.-butyl lithium; pyridinium p-toluenesulfonate; diisobutylaluminium hydride; 9-methoxy-9-BBN; triphenylphosphine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In tetrahydrofuran; diethyl ether; hexane; dichloromethane; water; acetonitrile; pentane; 5.1: Suzuki-Miyaura coupling / 5.2: Suzuki-Miyaura coupling;
DOI:10.1021/ja305864z

Reference yield:

: 1388153-35-2
C₂₄H₃₆O₃Si

: 1388153-00-1
C₄₈H₇₁BrO₇Si₂

Guidance literature:: Multi-step reaction with 6 steps

1.1: pyridinium p-toluenesulfonate / dichloromethane / 2 h / 20 °C

2.1: diisobutylaluminium hydride / hexane; dichloromethane / 2.5 h / -78 - -40 °C / Inert atmosphere

3.1: 1H-imidazole; iodine; triphenylphosphine / tetrahydrofuran / 0.5 h / 20 °C

4.1: tert.-butyl lithium; 9-methoxy-9-BBN / diethyl ether; hexane; pentane / 1.08 h / -78 - 20 °C / Inert atmosphere

4.2: 2 h / 50 °C / Inert atmosphere

5.1: Allyl ether; 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane / 1 h / 0 - 20 °C / pH 7 / aq. phosphate buffer

6.1: N-Bromosuccinimide / acetonitrile / 1 h / 0 - 20 °C

With 1H-imidazole; N-Bromosuccinimide; Allyl ether; iodine; tert.-butyl lithium; pyridinium p-toluenesulfonate; diisobutylaluminium hydride; 9-methoxy-9-BBN; triphenylphosphine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In tetrahydrofuran; diethyl ether; hexane; dichloromethane; acetonitrile; pentane; 4.1: Suzuki-Miyaura coupling / 4.2: Suzuki-Miyaura coupling;
DOI:10.1021/ja305864z