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C9H11F2NO

Base Information
  • Chemical Name:C9H11F2NO
  • CAS No.:254427-37-7
  • Molecular Formula:C9H11F2NO
  • Molecular Weight:187.189
  • Hs Code.:
C<sub>9</sub>H<sub>11</sub>F<sub>2</sub>NO

Synonyms:C9H11F2NO

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Chemical Property of C9H11F2NO
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Technology Process of C9H11F2NO

There total 1 articles about C9H11F2NO which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
2,5-difluoro-DL-phenylalanine; With lithium aluminium tetrahydride; In tetrahydrofuran; at 0 ℃; for 6h; Reflux;
With sodium hydroxide; In tetrahydrofuran; water;
Guidance literature:
In dichloromethane; at 20 ℃;
Guidance literature:
Multi-step reaction with 4 steps
1.1: dichloromethane / 20 °C
2.1: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran / 16 h / 0 °C
3.1: hydrazine hydrate / ethanol / 2 h / Reflux
4.1: dicyclohexyl-carbodiimide; benzotriazol-1-ol / dichloromethane / 1 h / 0 °C
4.2: 18 h / 20 °C
With benzotriazol-1-ol; hydrazine hydrate; dicyclohexyl-carbodiimide; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; ethanol; dichloromethane;
upstream raw materials:

2,5-difluoro-DL-phenylalanine

Downstream raw materials:

C14H19F2NO3

C20H31F2N3O3

C36H47BrF2N4O8

C36H48F2N4O9

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