(Rh₂(O₂CCHCl₂)(CO)2((C₆H₅)2PCH₂P(C₆H₅)2)2)⁽¹⁺⁾*ClO₄^(1-)=(Rh₂(O₂CCHCl₂)(CO)2((C₆H₅)2PCH₂P(C₆H₅)2)2)ClO₄

Base Information

• Chemical Name: (Rh₂(O₂CCHCl₂)(CO)2((C₆H₅)2PCH₂P(C₆H₅)2)2)⁽¹⁺⁾*ClO₄^(1-)=(Rh₂(O₂CCHCl₂)(CO)2((C₆H₅)2PCH₂P(C₆H₅)2)2)ClO₄
• CAS No.: 93683-47-7
• Molecular Formula: C₅₄H₄₅Cl₂O₄P₄Rh₂*ClO₄
• Molecular Weight: 1258.01

Synonyms:(Rh₂(O₂CCHCl₂)(CO)2((C₆H₅)2PCH₂P(C₆H₅)2)2)⁽¹⁺⁾*ClO₄^(1-)=(Rh₂(O₂CCHCl₂)(CO)2((C₆H₅)2PCH₂P(C₆H₅)2)2)ClO₄

Chemical Property of (Rh₂(O₂CCHCl₂)(CO)2((C₆H₅)2PCH₂P(C₆H₅)2)2)⁽¹⁺⁾*ClO₄^(1-)=(Rh₂(O₂CCHCl₂)(CO)2((C₆H₅)2PCH₂P(C₆H₅)2)2)ClO₄

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Technology Process of (Rh₂(O₂CCHCl₂)(CO)2((C₆H₅)2PCH₂P(C₆H₅)2)2)⁽¹⁺⁾*ClO₄^(1-)=(Rh₂(O₂CCHCl₂)(CO)2((C₆H₅)2PCH₂P(C₆H₅)2)2)ClO₄

There total 1 articles about (Rh₂(O₂CCHCl₂)(CO)2((C₆H₅)2PCH₂P(C₆H₅)2)2)⁽¹⁺⁾*ClO₄^(1-)=(Rh₂(O₂CCHCl₂)(CO)2((C₆H₅)2PCH₂P(C₆H₅)2)2)ClO₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

dichloro-acetic acid (79-43-6) + {Rh2(μ-OC2H5)(CO)2(μ-(C6h5)2PCH2P(C6H5)2)2}ClO4 (91581-10-1) → {Rh2(μ-OOCCHCl2)(CO)2(μ-(C6H5)2PCH2P(C6H5)2)2}ClO4 (93683-47-7)

Guidance literature:

In dichloromethane; a soln. of Rh-complex in CH2Cl2 was treated with CHCl2COOH under N2, Et2O was added;; recrystd. from CH2Cl2-Et2O;;

Reference yield: 88.0%

(Rh2(O2CCHCl2)(CO)2((C6H5)2PCH2P(C6H5)2)2)(1+)*ClO4(1-)=(Rh2(O2CCHCl2)(CO)2((C6H5)2PCH2P(C6H5)2)2)ClO4 (93683-47-7) → (Rh2(O2CCHCl2)(CO)3((C6H5)2PCH2P(C6H5)2)2)(1+)*ClO4(1-)=(Rh2(O2CCHCl2)(CO)3((C6H5)2PCH2P(C6H5)2)2)ClO4

Guidance literature:

With carbon monoxide; In dichloromethane; CO bubbled through soln. (Rh2(μ-O2CCHCl2)(CO)2(μ-dppm)2)ClO4 for 10 min; Et2O added, product filtered off, washed with Et2O and dried in air, recrystd. from CH2Cl2-Et2O in CO atm.;

DOI:10.1016/S0020-1693(00)85995-2

Reference yield: 85.0%

(Rh2(O2CCHCl2)(CO)2((C6H5)2PCH2P(C6H5)2)2)(1+)*ClO4(1-)=(Rh2(O2CCHCl2)(CO)2((C6H5)2PCH2P(C6H5)2)2)ClO4 (93683-47-7) → (Rh2(H)(CO)3((C6H5)2PCH2P(C6H5)2)2)(1+)*ClO4(1-)=(Rh2(H)(CO)3((C6H5)2PCH2P(C6H5)2)2)ClO4

Guidance literature:

With carbon monoxide; dihydrogen; In dichloromethane; mixt. CO/H2 (1:1) bubbled through soln. (Rh2(μ-O2CCHCl2)(CO)2(μ-dppm)2)ClO4 in CH2Cl2 for 5 min, flask capped under atm. reactant gas mixt and stirred for 0.75 h; Et2O added in CO atm., solid filtered and recrystd. from CH2Cl2-Et2O inpresence CO/N2;

DOI:10.1016/S0020-1693(00)85995-2

upstream raw materials:

dichloro-acetic acid

{Rh2(μ-OC2H5)(CO)2(μ-(C6h5)2PCH2P(C6H5)2)2}ClO4

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