(3aR,8aS)-7-phenethyloctahydropyrrolo[2,3-c]azepine-1-carboxylic acid benzyl ester

Base Information

Chemical Name:(3aR,8aS)-7-phenethyloctahydropyrrolo[2,3-c]azepine-1-carboxylic acid benzyl ester
CAS No.:1331846-69-5
Molecular Formula:C₂₄H₃₀N₂O₂
Molecular Weight:378.514
Hs Code.:

Synonyms:(3aR,8aS)-7-phenethyloctahydropyrrolo[2,3-c]azepine-1-carboxylic acid benzyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (3aR,8aS)-7-phenethyloctahydropyrrolo[2,3-c]azepine-1-carboxylic acid benzyl ester

Chemical Property:

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Technology Process of (3aR,8aS)-7-phenethyloctahydropyrrolo[2,3-c]azepine-1-carboxylic acid benzyl ester

There total 1 articles about (3aR,8aS)-7-phenethyloctahydropyrrolo[2,3-c]azepine-1-carboxylic acid benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 867326-49-6
(3aR,8aS)-7-phenethyl-decahydro-pyrrolo[2,3-c]azepine

: 501-53-1,94274-21-2
benzyl chloroformate

: 1331846-69-5
(3aR,8aS)-7-phenethyloctahydropyrrolo[2,3-c]azepine-1-carboxylic acid benzyl ester

Guidance literature:: With potassium carbonate; In water; ethyl acetate; at 0 - 23 ℃; for 3h;

Reference yield:

: 1331846-69-5
(3aR,8aS)-7-phenethyloctahydropyrrolo[2,3-c]azepine-1-carboxylic acid benzyl ester

: 1331846-70-8
(3aR,8aS)-octahydropyrrolo[2,3-c]azepine-1-carboxylic acid benzyl ester

Guidance literature:: (3aR,8aS)-7-phenethyloctahydropyrrolo[2,3-c]azepine-1-carboxylic acid benzyl ester; With carbonochloridic acid 1-chloro-ethyl ester; In 1,2-dichloro-ethane; at 0 - 23 ℃; for 4h; Reflux;

With methanol; In 1,2-dichloro-ethane; at 50 ℃; for 1h;

Reference yield:

: 1331846-69-5
(3aR,8aS)-7-phenethyloctahydropyrrolo[2,3-c]azepine-1-carboxylic acid benzyl ester

: C₃₆H₄₂N₈O₄

Guidance literature:: Multi-step reaction with 2 steps

1.1: carbonochloridic acid 1-chloro-ethyl ester / 1,2-dichloro-ethane / 4 h / 0 - 23 °C / Reflux

1.2: 1 h / 50 °C

2.1: triethylamine; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate / N,N-dimethyl-formamide / 0.08 h / 23 °C

2.2: 1.5 h / 23 °C

With carbonochloridic acid 1-chloro-ethyl ester; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; triethylamine; In 1,2-dichloro-ethane; N,N-dimethyl-formamide;