8,10-dibenzyl-8,10-diaza-5-<(phenylselenyl)methyl>-2-oxabicyclo<4.2.2>decane-7,9-dione

Base Information

Chemical Name:8,10-dibenzyl-8,10-diaza-5-<(phenylselenyl)methyl>-2-oxabicyclo<4.2.2>decane-7,9-dione
CAS No.:95782-42-6
Molecular Formula:C₂₈H₂₈N₂O₃Se
Molecular Weight:519.502
Hs Code.:

Synonyms:8,10-dibenzyl-8,10-diaza-5-<(phenylselenyl)methyl>-2-oxabicyclo<4.2.2>decane-7,9-dione

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Chemical Property of 8,10-dibenzyl-8,10-diaza-5-<(phenylselenyl)methyl>-2-oxabicyclo<4.2.2>decane-7,9-dione

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Technology Process of 8,10-dibenzyl-8,10-diaza-5-<(phenylselenyl)methyl>-2-oxabicyclo<4.2.2>decane-7,9-dione

There total 5 articles about 8,10-dibenzyl-8,10-diaza-5-<(phenylselenyl)methyl>-2-oxabicyclo<4.2.2>decane-7,9-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1666-13-3
diphenyl diselenide

: 95782-37-9
Methanesulfonic acid (1R,5R,6R)-7,9-dibenzyl-8,10-dioxo-2-oxa-7,9-diaza-bicyclo[4.2.2]dec-5-ylmethyl ester

: 95782-42-6
8,10-dibenzyl-8,10-diaza-5-<(phenylselenyl)methyl>-2-oxabicyclo<4.2.2>decane-7,9-dione

Guidance literature:: With sodium tetrahydroborate; In ethanol; at 45 ℃; for 0.333333h;
DOI:10.1021/ja00297a035

Reference yield:

: 95782-30-2
1,4-dibenzyl-3-(2'-thiopyridyl)-6-<1''-(hydroxymethyl)-3''-(hydroxypropyl)>-2,5-piperazinedione

: 95782-42-6
8,10-dibenzyl-8,10-diaza-5-<(phenylselenyl)methyl>-2-oxabicyclo<4.2.2>decane-7,9-dione

Guidance literature:: Multi-step reaction with 4 steps

1: 46 percent / DMAP, triethylamine / CH₂Cl₂ / 24 h / Ambient temperature

2: 98 percent / Et₃N / tetrahydrofuran / 0.17 h / Ambient temperature

3: 78 percent / PhHgClO₄ / tetrahydrofuran / 25 °C

4: NaBH₄ / ethanol / 0.33 h / 45 °C

With dmap; sodium tetrahydroborate; phenylmercuric perchlorate; triethylamine; In tetrahydrofuran; ethanol; dichloromethane;
DOI:10.1021/ja00297a035

Reference yield:

: 95782-34-6
1,4-dibenzyl-3-(2'-thiopyridyl)-6-<1''-<((methylsulfonyl)oxy)methyl>-3''-<((tert-butyldimethylsilyl)oxy)propyl>>-2,5-piperazinedione

: 95782-42-6
8,10-dibenzyl-8,10-diaza-5-<(phenylselenyl)methyl>-2-oxabicyclo<4.2.2>decane-7,9-dione

Guidance literature:: Multi-step reaction with 2 steps

1: 78 percent / PhHgClO₄ / tetrahydrofuran / 25 °C

2: NaBH₄ / ethanol / 0.33 h / 45 °C

With sodium tetrahydroborate; phenylmercuric perchlorate; In tetrahydrofuran; ethanol;
DOI:10.1021/ja00297a035