[Cu(chloride)2(2-(pyrimidin-2-ylamino)-1,3-thiazole-4-carbaldehyde)]2

Base Information

Chemical Name:[Cu(chloride)2(2-(pyrimidin-2-ylamino)-1,3-thiazole-4-carbaldehyde)]2
CAS No.:1269634-02-7
Molecular Formula:C₁₆H₁₂Cl₄Cu₂N₈O₂S₂
Molecular Weight:681.36
Hs Code.:

Synonyms:[Cu(chloride)2(2-(pyrimidin-2-ylamino)-1,3-thiazole-4-carbaldehyde)]2

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Chemical Property of [Cu(chloride)2(2-(pyrimidin-2-ylamino)-1,3-thiazole-4-carbaldehyde)]2

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Technology Process of [Cu(chloride)2(2-(pyrimidin-2-ylamino)-1,3-thiazole-4-carbaldehyde)]2

There total 2 articles about [Cu(chloride)2(2-(pyrimidin-2-ylamino)-1,3-thiazole-4-carbaldehyde)]2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: copper(II) choride dihydrate

: 15718-46-4
2,2'-dipyrimidyl disulfide

: 10544-50-0
sulfur

: 1269634-02-7
[Cu(chloride)2(2-(pyrimidin-2-ylamino)-1,3-thiazole-4-carbaldehyde)]2

Guidance literature:: In dichloromethane; acetonitrile; byproducts: SO4(2-); High Pressure; mixing Cu compd., S compd. in CH2Cl2/MeCN (1:1), stirring at room temp. for 30 min, sealing in autoclave, heating at 90°C for 20 h, various temp. (60 or 90°C), various times (1 h or 3-20 h); slow cooling (2.5°C/h) to ambient temp., isolation of crystals after storage at 0°C for 2 weeks, washing with Et2O, air drying, elem. anal.;
DOI:10.1039/c0dt00973c

Reference yield: 8.0%

: copper(II) choride dihydrate

: 15718-46-4
2,2'-dipyrimidyl disulfide

: 10544-50-0
sulfur

: 1269634-02-7
[Cu(chloride)2(2-(pyrimidin-2-ylamino)-1,3-thiazole-4-carbaldehyde)]2

: (9[Cu(bis(2-pyrimidyl)trisulfide)(chloride)2]2*[Cu(bis(2-pyrimidyl)disulfide)(chloride)2]2)

Guidance literature:: In dichloromethane; acetonitrile; byproducts: SO4(2-); other Radiation; mixing Cu compd., S compd. in CH2Cl2/MeCN (1:1), sealing in autoclave, irradiation in microwave oven (2*800 W, 2.45 GHz), heating to 90°Cin 20 min, storage for 1 h, various times (1 h or 3-20 h), various temp . (60 or 90°C); slow cooling to room temp. over 9 h, isolation of crystals after storageat 0°C for 2 weeks, manually separation of crystals, washing wit h Et2O, air drying, elem. anal.;
DOI:10.1039/c0dt00973c