Ethyl (1R^*,2S^*,3S^*)-2-Hydroxy-3-<(1-hydroxy-2-methylcyclohex-1-yl)methyl>-1,2-dimethylcyclopentanecarboxylate

Base Information

• Chemical Name: Ethyl (1R^*,2S^*,3S^*)-2-Hydroxy-3-<(1-hydroxy-2-methylcyclohex-1-yl)methyl>-1,2-dimethylcyclopentanecarboxylate
• CAS No.: 132102-97-7
• Molecular Formula: C₁₈H₃₂O₄
• Molecular Weight: 312.45

Synonyms:Ethyl (1R^*,2S^*,3S^*)-2-Hydroxy-3-<(1-hydroxy-2-methylcyclohex-1-yl)methyl>-1,2-dimethylcyclopentanecarboxylate

Chemical Property of Ethyl (1R^*,2S^*,3S^*)-2-Hydroxy-3-<(1-hydroxy-2-methylcyclohex-1-yl)methyl>-1,2-dimethylcyclopentanecarboxylate

Chemical Property:

Purity/Quality:

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Technology Process of Ethyl (1R^*,2S^*,3S^*)-2-Hydroxy-3-<(1-hydroxy-2-methylcyclohex-1-yl)methyl>-1,2-dimethylcyclopentanecarboxylate

There total 1 articles about Ethyl (1R^*,2S^*,3S^*)-2-Hydroxy-3-<(1-hydroxy-2-methylcyclohex-1-yl)methyl>-1,2-dimethylcyclopentanecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

2-acetyl-2-methyl-hex-5-enoic acid ethyl ester (54044-86-9) + 2-Methylcyclohexanone (583-60-8) → ethyl (1RS,2SR,3RS)-2-hydroxy-1,2,3-trimethylcyclopentanecarboxylate (29915-94-4,114761-41-0,123284-25-3) + Ethyl (1R*,2S*,3S*)-2-Hydroxy-3-<(1-hydroxy-2-methylcyclohex-1-yl)methyl>-1,2-dimethylcyclopentanecarboxylate (132102-97-7)

Guidance literature:

With samarium diiodide; In tetrahydrofuran; at 25 ℃; for 2h;

DOI:10.1021/jo00004a020

upstream raw materials:

2-acetyl-2-methyl-hex-5-enoic acid ethyl ester

2-Methylcyclohexanone

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