methyl hydrogen <<1(R)-1-N-<(phenylmethoxy)carbonyl>amino>-2-phenylethyl>phosphonate

Base Information

Chemical Name:methyl hydrogen <<1(R)-1-N-<(phenylmethoxy)carbonyl>amino>-2-phenylethyl>phosphonate
CAS No.:107133-12-0
Molecular Formula:C₁₇H₂₀NO₅P
Molecular Weight:349.323
Hs Code.:

Synonyms:methyl hydrogen <<1(R)-1-N-<(phenylmethoxy)carbonyl>amino>-2-phenylethyl>phosphonate

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Chemical Property of methyl hydrogen <<1(R)-1-N-<(phenylmethoxy)carbonyl>amino>-2-phenylethyl>phosphonate

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Technology Process of methyl hydrogen <<1(R)-1-N-<(phenylmethoxy)carbonyl>amino>-2-phenylethyl>phosphonate

There total 3 articles about methyl hydrogen <<1(R)-1-N-<(phenylmethoxy)carbonyl>amino>-2-phenylethyl>phosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 107133-10-8
(R)-benzyl N-[1-(dimethoxyphosphoryl)-2-phenylethyl]carbamate

: 107133-12-0
methyl hydrogen <<1(R)-1-N-<(phenylmethoxy)carbonyl>amino>-2-phenylethyl>phosphonate

Guidance literature:: With sodium hydroxide; In methanol;
DOI:10.1016/0968-0896(96)00085-5

Reference yield:

: C₁₇H₂₀NO₄P

: 107133-12-0
methyl hydrogen <<1(R)-1-N-<(phenylmethoxy)carbonyl>amino>-2-phenylethyl>phosphonate

Guidance literature:: With sodium periodate; In 1,4-dioxane; for 16h; Yield given; Ambient temperature;
DOI:10.1021/jo00121a045

Reference yield:

: (R)-<1-<(Benzyloxycarbonyl)amino>-2-phenylethyl>phosphonous acid

: 107133-12-0
methyl hydrogen <<1(R)-1-N-<(phenylmethoxy)carbonyl>amino>-2-phenylethyl>phosphonate

Guidance literature:: Multi-step reaction with 2 steps

1: DCC, DMAP / tetrahydrofuran / 24 h / Ambient temperature

2: aq. NaIO₄ / dioxane / 16 h / Ambient temperature

With dmap; sodium periodate; dicyclohexyl-carbodiimide; In tetrahydrofuran; 1,4-dioxane;
DOI:10.1021/jo00121a045