N-(2-(1-benzyl-2-oxoindolin-3-yl)ethyl)-N,4-dimethylbenzenesulfonamide

Base Information

Chemical Name:N-(2-(1-benzyl-2-oxoindolin-3-yl)ethyl)-N,4-dimethylbenzenesulfonamide
CAS No.:1448522-97-1
Molecular Formula:C₂₅H₂₆N₂O₃S
Molecular Weight:434.559
Hs Code.:

Synonyms:N-(2-(1-benzyl-2-oxoindolin-3-yl)ethyl)-N,4-dimethylbenzenesulfonamide

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Chemical Property of N-(2-(1-benzyl-2-oxoindolin-3-yl)ethyl)-N,4-dimethylbenzenesulfonamide

Chemical Property:

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Technology Process of N-(2-(1-benzyl-2-oxoindolin-3-yl)ethyl)-N,4-dimethylbenzenesulfonamide

There total 4 articles about N-(2-(1-benzyl-2-oxoindolin-3-yl)ethyl)-N,4-dimethylbenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 44.0%

: 857776-34-2
N-(2-(1-benzyl-1H-indol-3-yl)ethyl)-N,4-dimethylbenzenesulfonamide

: 1448522-97-1
N-(2-(1-benzyl-2-oxoindolin-3-yl)ethyl)-N,4-dimethylbenzenesulfonamide

Guidance literature:: With N-Bromosuccinimide; water; In tetrahydrofuran; tert-butyl alcohol; at 20 ℃; for 2.5h;
DOI:10.1002/chem.201203150

Reference yield:

: 61-49-4
[2-(1H-indol-3-yl)-ethyl]-methylamine

: 1448522-97-1
N-(2-(1-benzyl-2-oxoindolin-3-yl)ethyl)-N,4-dimethylbenzenesulfonamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: triethylamine; dmap / dichloromethane / 6 h / 0 - 20 °C / Inert atmosphere

2.1: sodium hydride / mineral oil; N,N-dimethyl-formamide / 0.33 h / 20 °C

2.2: 3 h / 20 °C / Inert atmosphere

3.1: water; N-Bromosuccinimide / tetrahydrofuran; tert-butyl alcohol / 2.5 h / 20 °C

With dmap; N-Bromosuccinimide; water; sodium hydride; triethylamine; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; mineral oil; tert-butyl alcohol;
DOI:10.1002/chem.201203150

Reference yield:

: 442531-80-8
N-(2-(1H-indol-3-yl)ethyl)-N,4-dimethylbenzenesulfonamide

: 1448522-97-1
N-(2-(1-benzyl-2-oxoindolin-3-yl)ethyl)-N,4-dimethylbenzenesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / mineral oil; N,N-dimethyl-formamide / 0.33 h / 20 °C

1.2: 3 h / 20 °C / Inert atmosphere

2.1: water; N-Bromosuccinimide / tetrahydrofuran; tert-butyl alcohol / 2.5 h / 20 °C

With N-Bromosuccinimide; water; sodium hydride; In tetrahydrofuran; N,N-dimethyl-formamide; mineral oil; tert-butyl alcohol;
DOI:10.1002/chem.201203150