1-((4S,6S)-6-[(3S)-3-([(tert-butyl)diphenylsilyl]oxy)heptadecyl]-2,2-dimethyl-1,3-dioxan-4-yl)-4-penten-2-one

Base Information

Chemical Name:1-((4S,6S)-6-[(3S)-3-([(tert-butyl)diphenylsilyl]oxy)heptadecyl]-2,2-dimethyl-1,3-dioxan-4-yl)-4-penten-2-one
CAS No.:1263876-06-7
Molecular Formula:C₄₄H₇₀O₄Si
Molecular Weight:691.123
Hs Code.:

Synonyms:1-((4S,6S)-6-[(3S)-3-([(tert-butyl)diphenylsilyl]oxy)heptadecyl]-2,2-dimethyl-1,3-dioxan-4-yl)-4-penten-2-one

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Chemical Property of 1-((4S,6S)-6-[(3S)-3-([(tert-butyl)diphenylsilyl]oxy)heptadecyl]-2,2-dimethyl-1,3-dioxan-4-yl)-4-penten-2-one

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Technology Process of 1-((4S,6S)-6-[(3S)-3-([(tert-butyl)diphenylsilyl]oxy)heptadecyl]-2,2-dimethyl-1,3-dioxan-4-yl)-4-penten-2-one

There total 1 articles about 1-((4S,6S)-6-[(3S)-3-([(tert-butyl)diphenylsilyl]oxy)heptadecyl]-2,2-dimethyl-1,3-dioxan-4-yl)-4-penten-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 1263876-12-5
C₄₄H₇₂O₄Si

: 1263876-06-7
1-((4S,6S)-6-[(3S)-3-([(tert-butyl)diphenylsilyl]oxy)heptadecyl]-2,2-dimethyl-1,3-dioxan-4-yl)-4-penten-2-one

Guidance literature:: With Dess-Martin periodane; In dichloromethane; at 20 ℃; for 1h;
DOI:10.1055/s-0030-1258253

Reference yield: 86.0%

: 1263876-06-7
1-((4S,6S)-6-[(3S)-3-([(tert-butyl)diphenylsilyl]oxy)heptadecyl]-2,2-dimethyl-1,3-dioxan-4-yl)-4-penten-2-one

: 1263876-07-8
(2R)-1-((4R,6S)-6-[(3S)-3-([(tert-butyl)diphenylsilyl]oxy)heptadecyl]-2,2-dimethyl-1,3-dioxan-4-yl)-4-penten-2-ol

Guidance literature:: 1-((4S,6S)-6-[(3S)-3-([(tert-butyl)diphenylsilyl]oxy)heptadecyl]-2,2-dimethyl-1,3-dioxan-4-yl)-4-penten-2-one; With lithium iodide; In diethyl ether; at -40 ℃; for 0.5h; Inert atmosphere; Large scale reaction;

With lithium aluminium tetrahydride; In diethyl ether; at -100 - 0 ℃; stereoselective reaction;
DOI:10.1055/s-0030-1258253