Technology Process of hexane
There total 5 articles about hexane which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
C19H19N3O4S;
With
thiophene; hydrogen;
palladium 10% on activated carbon; vanadium(V) oxide;
In
tetrahydrofuran; di-isopropyl ether;
at 20 ℃;
3,4,5,6-tetrahydro-2H-pyran-4-carbaldehyde;
With
sodium cyanoborohydride; acetic acid;
In
tetrahydrofuran; methanol; di-isopropyl ether;
- Guidance literature:
-
C19H19N3O4S;
With
vanadium pentoxide; palladium 10% on activated carbon; hydrogen;
In
tetrahydrofuran; thiophene; di-isopropyl ether;
3,4,5,6-tetrahydro-2H-pyran-4-carbaldehyde;
With
acetic acid;
In
tetrahydrofuran; thiophene; methanol; di-isopropyl ether;
for 0.166667h;
Inert atmosphere;
With
sodium cyanoborohydride;
In
tetrahydrofuran; thiophene; methanol; di-isopropyl ether;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: potassium hydroxide / ethanol / 2 h / Reflux
2.1: phosphorus trichloride / pyridine / 0 - 20 °C / Inert atmosphere
3.1: vanadium pentoxide; hydrogen; palladium 10% on activated carbon / tetrahydrofuran; thiophene; di-isopropyl ether
3.2: 0.17 h / Inert atmosphere
With
vanadium pentoxide; palladium 10% on activated carbon; hydrogen; potassium hydroxide; phosphorus trichloride;
In
tetrahydrofuran; thiophene; pyridine; ethanol; di-isopropyl ether;
