N^α,N^ε-bis(hexadecyloxycarbonyl)-N-[2-(benzyloxycarbonyl)ethyl]-L-lysinamide

Base Information

Chemical Name:N^α,N^ε-bis(hexadecyloxycarbonyl)-N-[2-(benzyloxycarbonyl)ethyl]-L-lysinamide
CAS No.:258875-34-2
Molecular Formula:C₅₀H₈₉N₃O₇
Molecular Weight:844.273
Hs Code.:

N<sup>α</sup>,N<sup>ε</sup>-bis(hexadecyloxycarbonyl)-N-[2-(benzyloxycarbonyl)ethyl]-L-lysinamide

Synonyms:N^α,N^ε-bis(hexadecyloxycarbonyl)-N-[2-(benzyloxycarbonyl)ethyl]-L-lysinamide

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Chemical Property of N^α,N^ε-bis(hexadecyloxycarbonyl)-N-[2-(benzyloxycarbonyl)ethyl]-L-lysinamide

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Technology Process of N^α,N^ε-bis(hexadecyloxycarbonyl)-N-[2-(benzyloxycarbonyl)ethyl]-L-lysinamide

There total 3 articles about N^α,N^ε-bis(hexadecyloxycarbonyl)-N-[2-(benzyloxycarbonyl)ethyl]-L-lysinamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 27019-47-2
β-alanine benzyl ester p-toluenesulfonate

: 258875-26-2
N^α,N^ε-bis(hexadecyloxycarbonyl)-L-lysine

: 258875-34-2
N^α,N^ε-bis(hexadecyloxycarbonyl)-N-[2-(benzyloxycarbonyl)ethyl]-L-lysinamide

Guidance literature:: With diethyl cyanophosphonate; triethylamine; In tetrahydrofuran; chloroform; at 20 ℃; for 24h;
DOI:10.1039/a903956b

Reference yield:

: 26272-90-2
cetyl chloroformate

: 258875-34-2
N^α,N^ε-bis(hexadecyloxycarbonyl)-N-[2-(benzyloxycarbonyl)ethyl]-L-lysinamide

Guidance literature:: Multi-step reaction with 2 steps

1: 62 percent / NaOH / H₂O; acetone / 48 h

2: 77 percent / triethylamine; diethyl cyanophosphonate / CHCl₃; tetrahydrofuran / 24 h / 20 °C

With sodium hydroxide; diethyl cyanophosphonate; triethylamine; In tetrahydrofuran; chloroform; water; acetone; 1: Acylation / 2: Acylation;
DOI:10.1039/a903956b

Reference yield:

: 657-27-2,10098-89-2,26124-78-7
L-Lysine hydrochloride

: 258875-34-2
N^α,N^ε-bis(hexadecyloxycarbonyl)-N-[2-(benzyloxycarbonyl)ethyl]-L-lysinamide

Guidance literature:: Multi-step reaction with 2 steps

1: 62 percent / NaOH / H₂O; acetone / 48 h

2: 77 percent / triethylamine; diethyl cyanophosphonate / CHCl₃; tetrahydrofuran / 24 h / 20 °C

With sodium hydroxide; diethyl cyanophosphonate; triethylamine; In tetrahydrofuran; chloroform; water; acetone; 1: Acylation / 2: Acylation;
DOI:10.1039/a903956b