(2R,5R,2'R)-5-(hydroxymethyl)-2-[3'-(4-methoxybenzyloxy)-2'-methylpropyl]-2-methyltetrahydrofuran

Base Information

• Chemical Name: (2R,5R,2'R)-5-(hydroxymethyl)-2-[3'-(4-methoxybenzyloxy)-2'-methylpropyl]-2-methyltetrahydrofuran
• CAS No.: 1108185-77-8
• Molecular Formula: C₁₈H₂₈O₄
• Molecular Weight: 308.418

Synonyms:(2R,5R,2'R)-5-(hydroxymethyl)-2-[3'-(4-methoxybenzyloxy)-2'-methylpropyl]-2-methyltetrahydrofuran

Chemical Property of (2R,5R,2'R)-5-(hydroxymethyl)-2-[3'-(4-methoxybenzyloxy)-2'-methylpropyl]-2-methyltetrahydrofuran

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Technology Process of (2R,5R,2'R)-5-(hydroxymethyl)-2-[3'-(4-methoxybenzyloxy)-2'-methylpropyl]-2-methyltetrahydrofuran

There total 1 articles about (2R,5R,2'R)-5-(hydroxymethyl)-2-[3'-(4-methoxybenzyloxy)-2'-methylpropyl]-2-methyltetrahydrofuran which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

(2R,5R,2'R)-5-(iodomethyl)-2-[3'-(4-methoxybenzyloxy)-2'-methylpropyl]-2-methyltetrahydrofuran (1108185-64-3) → (2R,5R,2'R)-5-(hydroxymethyl)-2-[3'-(4-methoxybenzyloxy)-2'-methylpropyl]-2-methyltetrahydrofuran (1108185-77-8)

Guidance literature:

With potassium superoxide; 18-crown-6 ether; In tetrahydrofuran; dimethyl sulfoxide; at 20 ℃; Inert atmosphere;

DOI:10.1021/ol8025457

Reference yield: 71.0%

(2R,5R,2'R)-5-(hydroxymethyl)-2-[3'-(4-methoxybenzyloxy)-2'-methylpropyl]-2-methyltetrahydrofuran (1108185-77-8) → (2R,5R,2'R)-5-(formyl)-2-[3'-(4-methoxybenzyloxy)-2'-methylpropyl]-2-methyltetrahydrofuran (1108185-46-1)

Guidance literature:

With pyridine; Dess-Martin periodane; In dichloromethane; at 20 ℃; for 2h; Inert atmosphere;

DOI:10.1021/ol8025457

upstream raw materials:

(2R,5R,2'R)-5-(iodomethyl)-2-[3'-(4-methoxybenzyloxy)-2'-methylpropyl]-2-methyltetrahydrofuran

Downstream raw materials:

(2R,5R,2'R)-5-(formyl)-2-[3'-(4-methoxybenzyloxy)-2'-methylpropyl]-2-methyltetrahydrofuran

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