Technology Process of C33H35N2O7(1+)*Cl(1-)
There total 7 articles about C33H35N2O7(1+)*Cl(1-) which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
C41H51N2O7(1+)*Cl(1-);
With
trifluoroacetic acid;
In
dichloromethane;
at 25 ℃;
for 1h;
In
methanol; dichloromethane;
at 20 ℃;
DOI:10.1021/jo800902j
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: pyridine / dichloromethane / 0.25 h / 0 °C
1.2: 24 h / 0 - 20 °C
2.1: dimethyl sulfoxide / 12 h / 90 °C
3.1: tetrahydrofuran / 12 h / 0 - 20 °C
3.2: 0.17 h
4.1: boron tribromide / dichloromethane / -78 - 20 °C
4.2: Amberlite IRA-400 (CI) ion exchange resin / 1 h / 20 °C
5.1: caesium carbonate; tetra-(n-butyl)ammonium iodide / N,N-dimethyl-formamide / 12 h / 25 °C
6.1: trifluoroacetic acid / dichloromethane / 1 h / 25 °C
With
pyridine; boron tribromide; tetra-(n-butyl)ammonium iodide; caesium carbonate; trifluoroacetic acid;
In
tetrahydrofuran; dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 7 steps
1.1: water / 6 h / 200 °C / Autoclave
2.1: pyridine / dichloromethane / 0.25 h / 0 °C
2.2: 24 h / 0 - 20 °C
3.1: dimethyl sulfoxide / 12 h / 90 °C
4.1: tetrahydrofuran / 12 h / 0 - 20 °C
4.2: 0.17 h
5.1: boron tribromide / dichloromethane / -78 - 20 °C
5.2: Amberlite IRA-400 (CI) ion exchange resin / 1 h / 20 °C
6.1: caesium carbonate; tetra-(n-butyl)ammonium iodide / N,N-dimethyl-formamide / 12 h / 25 °C
7.1: trifluoroacetic acid / dichloromethane / 1 h / 25 °C
With
pyridine; boron tribromide; tetra-(n-butyl)ammonium iodide; caesium carbonate; trifluoroacetic acid;
In
tetrahydrofuran; dichloromethane; water; dimethyl sulfoxide; N,N-dimethyl-formamide;