PROPYLMAGNESIUM CHLORIDE

Base Information

• Chemical Name: PROPYLMAGNESIUM CHLORIDE
• CAS No.: 2234-82-4
• Molecular Formula: C3H7ClMg
• Molecular Weight: 102.847
• Hs Code.: 29319090
• Mol file: 2234-82-4.mol

Synonyms:Propylmagnesiumchloride (6CI);Chloropropylmagnesium;n-Propylmagnesium chloride;

Chemical Property of PROPYLMAGNESIUM CHLORIDE

Chemical Property:

• Boiling Point: 148-150 °C(Press: 15 Torr)
• Flash Point: -40 °c
• PSA: 0.00000
• Density: 0.83 g/mL at 20 °C
• LogP: 2.05350
• Sensitive.: Air & Moisture Sensitive
• Water Solubility.: Reacts with water.

Purity/Quality:

99% ^*data from raw suppliers

n-Propylmagnesium chloride solution 1.0 M in 2-methyltetrahydrofuran ^*data from reagent suppliers

Safty Information:

• Pictogram(s): F+; C
• Hazard Codes: F+,C,F
• Statements: 12-14/15-22-34-66-67-19-11
• Safety Statements: 16-26-36/37/39-43-45-7/8

MSDS Files:

SDS file from LookChem

Useful:

• Uses: Propylmagnesium Chloride is a useful reagent for the preparation of 4-(2,4-bis(2-Hydroxyphenyl)-1H-imidazol-1-yl)benzoic Acid derivatives as novel iron chelators. Grignard reagent in greener solvent, 2-methyltetrahydrofuran (2-MeTHF)2-Methyltetrahydrofuran (2-MeTHF): A Biomass-Derived Solvent with Broad Application in Organic Chemistry

Technology Process of PROPYLMAGNESIUM CHLORIDE

There total 4 articles about PROPYLMAGNESIUM CHLORIDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

→ 9-bromonon-4-yne (81168-90-3) + 1-propylmagnesium chloride (2234-82-4)

Guidance literature:

Reference yield:

1-Chloropropane (540-54-5) → 1-propylmagnesium chloride (2234-82-4)

Guidance literature:

With magnesium; In tetrahydrofuran;

Reference yield:

1-Chloropropane (540-54-5) → 1-propylmagnesium chloride (2234-82-4)

Guidance literature:

With diethyl ether;

upstream raw materials:

1-Chloropropane

Downstream raw materials:

butyraldehyde

3,3-dimethyl-2-butanol

2,2,3-trimethyl-hexan-3-ol

3,5,5-trimethyl-1-propyl-cyclohex-2-enol

Refernces

• 1、 -. "Sulphur-containing eicosanoides and their application in pharmacy and in cosmetics". . . Retrieved 2008/06/13.
• 2、 -. "Coupling reaction involving a Grignard and allylic halide". . . Retrieved 2008/06/13.