cis-diaqua-bis-(2-(m-tolylazo)pyridine)ruthenium(II) diperchlorate monohydrate

Base Information

Chemical Name:cis-diaqua-bis-(2-(m-tolylazo)pyridine)ruthenium(II) diperchlorate monohydrate
CAS No.:84049-25-2
Molecular Formula:C₂₄H₂₆N₆O₂Ru*2ClO₄*H₂O
Molecular Weight:748.496
Hs Code.:

Synonyms:cis-diaqua-bis-(2-(m-tolylazo)pyridine)ruthenium(II) diperchlorate monohydrate

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Chemical Property of cis-diaqua-bis-(2-(m-tolylazo)pyridine)ruthenium(II) diperchlorate monohydrate

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Technology Process of cis-diaqua-bis-(2-(m-tolylazo)pyridine)ruthenium(II) diperchlorate monohydrate

There total 1 articles about cis-diaqua-bis-(2-(m-tolylazo)pyridine)ruthenium(II) diperchlorate monohydrate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: cis,cis-RuCl₂(2-(m-toylazo)pyridine)2

: silver perchlorate

: 84049-25-2
cis-diaqua-bis-(2-(m-tolylazo)pyridine)ruthenium(II) diperchlorate monohydrate

Guidance literature:: With H₂O; In water; byproducts: AgCl; to suspn. of complex in water AgClO4 added, mixt. refluxed for 2 h; cooled to room temp., filtered, excess of NaClO4 and 70% aq. HClO4 added, crystals filtered, dissolved in boilinf water, filtered hot, kept in refrigerator for 24 h, filtered, dried in vac. over P4O10; elem. anal.;

Reference yield: 65.0%

: 84049-25-2
cis-diaqua-bis-(2-(m-tolylazo)pyridine)ruthenium(II) diperchlorate monohydrate

: 86707-54-2
cc-(bipyridine)bis[2-(m-tolylazo)pyridine]ruthenium(II) perchlorate monohydrate

Guidance literature:: With sodium perchlorate; 2,2'-bipyridine; In methanol; to soln. of Ru complex was added ligand; refluxing for 1 h, adding of NaClO4 to hot soln.; keeping in refrigerator for 12 h; filtration, washing with water and MeOH, recrystn. from MeOH; filtration, drying in vac. over P4O10; elem. anal.;

Reference yield:

: 84049-25-2
cis-diaqua-bis-(2-(m-tolylazo)pyridine)ruthenium(II) diperchlorate monohydrate

: cis,cis-RuCl₂(2-(m-toylazo)pyridine)2

Guidance literature:: With LiCl; In water; to soln. of complex in water excess of LiCl added, soln. stirred at 40 °C for 1 h; ext. with CHCl3, evapd.;